Piperidine, 3-(4-broMophenyl)-, hydrochloride

Base Information

• Chemical Name: Piperidine, 3-(4-broMophenyl)-, hydrochloride
• CAS No.: 1203683-26-4
• Molecular Formula: C₁₁H₁₄BrN*ClH
• Molecular Weight: 276.604
• Mol file: 1203683-26-4.mol

Synonyms:Piperidine, 3-(4-broMophenyl)-, hydrochloride;3-(4-Bromo-phenyl)-piperidine hydrochloride

Chemical Property of Piperidine, 3-(4-broMophenyl)-, hydrochloride

Chemical Property:

• PSA: 12.03000
• LogP: 4.04690

Purity/Quality:

98% ^*data from raw suppliers

3-(4-Brombo-phenyl)piperidineHydrochloride ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Piperidine, 3-(4-broMophenyl)-, hydrochloride

There total 5 articles about Piperidine, 3-(4-broMophenyl)-, hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3-(4-bromophenyl)piperidine hydrochloride (1203683-26-4) → (S)-3-(4-bromophenyl)-piperidine hydrochloride (1203683-26-4) + (R)-3-(4-bromophenyl)piperidine hydrochloride (1203683-26-4)

Guidance literature:

With trifluoroacetic acid; In water; acetonitrile; Resolution of racemate;

Reference yield:

3-(4-bromophenyl)piperidine hydrochloride (1203683-26-4) → (S)-3-(4-bromophenyl)-piperidine hydrochloride (1203683-26-4) + (R)-3-(4-bromophenyl)piperidine hydrochloride (1203683-26-4)

Guidance literature:

With trifluoroacetic acid; In water; acetonitrile; Resolution of racemate;

Reference yield:

(S)-N-tert-butylsulfinyl-2-(4-bromophenyl)-1-methoxyethane-1-imine → (S)-3-(4-bromophenyl)-piperidine hydrochloride (1203683-26-4)

Guidance literature:

Multi-step reaction with 3 steps

1.1: lithium hexamethyldisilazane / tetrahydrofuran / 2 h / -70 - -65 °C / Inert atmosphere

1.2: 2 h / -70 - -65 °C

1.3: 2 h / 60 - 65 °C

2.1: sodium hydride / dimethyl sulfoxide / 2 h / 80 - 85 °C

3.1: hydrogenchloride / ethanol / 0.5 h

With hydrogenchloride; sodium hydride; lithium hexamethyldisilazane; In tetrahydrofuran; ethanol; dimethyl sulfoxide;

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