Pyrocatechol, 3-methyl-5-phenyl- (7CI)

Base Information

• Chemical Name: Pyrocatechol, 3-methyl-5-phenyl- (7CI)
• CAS No.: 95913-42-1
• Molecular Formula: C13H12O2
• Molecular Weight: 200.23318
• Mol file: 95913-42-1.mol

Synonyms:Pyrocatechol, 3-methyl-5-phenyl- (7CI)

Chemical Property of Pyrocatechol, 3-methyl-5-phenyl- (7CI)

Chemical Property:

• Melting Point: 109.5 - 110 °C (petroleum ether)
• PSA: 40.46000
• LogP: 3.07320

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Pyrocatechol, 3-methyl-5-phenyl- (7CI)

There total 5 articles about Pyrocatechol, 3-methyl-5-phenyl- (7CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-Chlor-6-methyl-4-phenylphenol (92023-25-1) → 3-Methyl-5-phenyl-brenzcatechin (95913-42-1)

Guidance literature:

With barium dihydroxide; sodium hydroxide; copper(II) sulfate; at 200 ℃;

DOI:10.1021/jo01032a040

Reference yield:

5-morpholin-4-ylmethyl-biphenyl-3,4-diol (6452-85-3) → 3-Methyl-5-phenyl-brenzcatechin (95913-42-1)

Guidance literature:

With hydrogen; palladium on activated charcoal;

DOI:10.1021/jo01032a040

Reference yield:

2-Morpholinomethyl-4-phenylphenol (6452-87-5) → 3-Methyl-5-phenyl-brenzcatechin (95913-42-1)

Guidance literature:

Multi-step reaction with 3 steps

1: H₂ / Pd-C

2: Cl₂

3: aq. NaOH, Ba(OH)2, CuSO₄ / 200 °C

With barium dihydroxide; sodium hydroxide; hydrogen; chlorine; copper(II) sulfate; palladium on activated charcoal;

DOI:10.1021/jo01032a040

upstream raw materials:

2-Chlor-6-methyl-4-phenylphenol

5-morpholin-4-ylmethyl-biphenyl-3,4-diol

2-Morpholinomethyl-4-phenylphenol

3-methyl-[1,1'-biphenyl]-4-ol