TERT-BUTYL [2-PHTHALIMIDO-1-(METHYLSULFANYLMETHYL)ETHYL]CARBAMATE

Base Information

• Chemical Name: TERT-BUTYL [2-PHTHALIMIDO-1-(METHYLSULFANYLMETHYL)ETHYL]CARBAMATE
• CAS No.: 885266-58-0
• Molecular Formula: C₁₇H₂₂N₂O₄S
• Molecular Weight: 350.439
• Hs Code.: 2930909090
• Mol file: 885266-58-0.mol

Synonyms:TERT-BUTYL [2-PHTHALIMIDO-1-(METHYLSULFANYLMETHYL)ETHYL]CARBAMATE

Chemical Property of TERT-BUTYL [2-PHTHALIMIDO-1-(METHYLSULFANYLMETHYL)ETHYL]CARBAMATE

Chemical Property:

• PSA: 101.01000
• LogP: 2.86770

Purity/Quality:

tert-Butyl [2-phthalimido-1-(methylsulfanylmethyl)-ethyl]carbamate ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of TERT-BUTYL [2-PHTHALIMIDO-1-(METHYLSULFANYLMETHYL)ETHYL]CARBAMATE

There total 3 articles about TERT-BUTYL [2-PHTHALIMIDO-1-(METHYLSULFANYLMETHYL)ETHYL]CARBAMATE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

phthalimide (136918-14-4,85-41-6) + tert-butyl [1-hydroxy-3-(methylsulfanyl)propan-2-yl]carbamate (1429913-61-0) → tert-butyl [1-(1,3-dioxo-1,3-dihydro-2H-isoindol-2-yl)-3-(methylsulfanyl)propan-2-yl]carbamate (885266-58-0)

Guidance literature:

With triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; at 20 ℃; for 2h; Inert atmosphere;

Reference yield:

N-(tert-butoxycarbonyl)-S-methyl-L-cysteine (16947-80-1) → tert-butyl [1-(1,3-dioxo-1,3-dihydro-2H-isoindol-2-yl)-3-(methylsulfanyl)propan-2-yl]carbamate (885266-58-0)

Guidance literature:

Multi-step reaction with 3 steps

1: triethylamine / tetrahydrofuran / 0.5 h / -10 °C

2: sodium tetrahydroborate / methanol / 2 h / 0 - 20 °C

3: triphenylphosphine; diethylazodicarboxylate / tetrahydrofuran / 2 h / 20 °C / Inert atmosphere

With sodium tetrahydroborate; triethylamine; triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; methanol;

Reference yield:

ethoxycarbonyl N-(tert-butoxycarbonyl)-S-methylcysteinate → tert-butyl [1-(1,3-dioxo-1,3-dihydro-2H-isoindol-2-yl)-3-(methylsulfanyl)propan-2-yl]carbamate (885266-58-0)

Guidance literature:

Multi-step reaction with 2 steps

1: sodium tetrahydroborate / methanol / 2 h / 0 - 20 °C

2: triphenylphosphine; diethylazodicarboxylate / tetrahydrofuran / 2 h / 20 °C / Inert atmosphere

With sodium tetrahydroborate; triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; methanol;

upstream raw materials:

N-(tert-butoxycarbonyl)-S-methyl-L-cysteine

phthalimide

tert-butyl [1-hydroxy-3-(methylsulfanyl)propan-2-yl]carbamate

Downstream raw materials:

tert-butyl [1-amino-3-(methylsulfanyl)propan-2-yl]carbamate

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