4'-IODO-2-(2-METHOXYPHENYL)ACETOPHENONE

Base Information

• Chemical Name: 4'-IODO-2-(2-METHOXYPHENYL)ACETOPHENONE
• CAS No.: 898784-93-5
• Molecular Formula: C15H13IO2
• Molecular Weight: 352.172
• Mol file: 898784-93-5.mol

Synonyms:4'-IODO-2-(2-METHOXYPHENYL)ACETOPHENONE

Chemical Property of 4'-IODO-2-(2-METHOXYPHENYL)ACETOPHENONE

Chemical Property:

• Vapor Pressure: 2.02E-07mmHg at 25°C
• Boiling Point: 424.7°C at 760 mmHg
• Flash Point: 210.7°C
• PSA: 26.30000
• Density: 1.546g/cm³
• LogP: 3.72520

Purity/Quality:

95% ^*data from raw suppliers

4'-iodo-2-(2-methoxyphenyl)acetophenone 97% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 4'-IODO-2-(2-METHOXYPHENYL)ACETOPHENONE

There total 2 articles about 4'-IODO-2-(2-METHOXYPHENYL)ACETOPHENONE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C16H13IO3 (1548157-88-5) → 1-(4-iodophenyl)-2-(2-methoxyphenyl)ethanone (898784-93-5)

Guidance literature:

With ethylenediamine; In dichloromethane; at 25 ℃;

DOI:10.1016/j.tet.2013.12.050

Reference yield:

C16H13IO3 (1542581-12-3) → 1-(4-iodophenyl)-2-(2-methoxyphenyl)ethanone (898784-93-5)

Guidance literature:

Multi-step reaction with 2 steps

1: boron trifluoride diethyl etherate / dichloromethane / 0.08 h / 25 °C

2: ethylenediamine / dichloromethane / 25 °C

With boron trifluoride diethyl etherate; ethylenediamine; In dichloromethane;

DOI:10.1016/j.tet.2013.12.050

Reference yield: 96.0%

1-(4-iodophenyl)-2-(2-methoxyphenyl)ethanone (898784-93-5) → 2-(4-iodophenyl)benzo[b]furan (1439923-28-0)

Guidance literature:

With hydrogen bromide; In acetic acid; for 8h; Reflux;

DOI:10.1016/j.tet.2013.12.050

upstream raw materials:

C₁₆H₁₃IO₃

C₁₆H₁₃IO₃

Downstream raw materials:

2-(4-iodophenyl)benzo[b]furan

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