ETHANESULFONIC ACID, 2-[(CYCLOHEXYLMETHYL)[(PHENYLMETHOXY)CARBONYL]AMINO]-1-HYDROXY-, SODIUM SALT (1:1)

Base Information

Chemical Name:ETHANESULFONIC ACID, 2-[(CYCLOHEXYLMETHYL)[(PHENYLMETHOXY)CARBONYL]AMINO]-1-HYDROXY-, SODIUM SALT (1:1)
CAS No.:949903-23-5
Molecular Formula:C17H24NNaO6S
Molecular Weight:393.436
Hs Code.:

Synonyms:ETHANESULFONIC ACID, 2-[(CYCLOHEXYLMETHYL)[(PHENYLMETHOXY)CARBONYL]AMINO]-1-HYDROXY-, SODIUM SALT (1:1)

Suppliers and Price of ETHANESULFONIC ACID, 2-[(CYCLOHEXYLMETHYL)[(PHENYLMETHOXY)CARBONYL]AMINO]-1-HYDROXY-, SODIUM SALT (1:1)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of ETHANESULFONIC ACID, 2-[(CYCLOHEXYLMETHYL)[(PHENYLMETHOXY)CARBONYL]AMINO]-1-HYDROXY-, SODIUM SALT (1:1)

Chemical Property:

PSA：115.35000
LogP:3.14990

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of ETHANESULFONIC ACID, 2-[(CYCLOHEXYLMETHYL)[(PHENYLMETHOXY)CARBONYL]AMINO]-1-HYDROXY-, SODIUM SALT (1:1)

There total 3 articles about ETHANESULFONIC ACID, 2-[(CYCLOHEXYLMETHYL)[(PHENYLMETHOXY)CARBONYL]AMINO]-1-HYDROXY-, SODIUM SALT (1:1) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 949903-24-6
N-cyclohexylmethyl-(2,2-diethoxyethyl)carbamic acid benzyl ester

: sodium hydrogensulfite

: 949903-23-5
N-cyclohexylmethyl-(2-oxoethyl)carbamic acid benzyl ester bisulfite adduct

Guidance literature:: N-cyclohexylmethyl-(2,2-diethoxyethyl)carbamic acid benzyl ester; With hydrogenchloride; In water; acetonitrile; at 30 ℃; for 7h;

sodium hydrogensulfite; In ethyl acetate; acetonitrile;

Reference yield:

: 949903-24-6
N-cyclohexylmethyl-(2,2-diethoxyethyl)carbamic acid benzyl ester

: 949903-23-5
N-cyclohexylmethyl-(2-oxoethyl)carbamic acid benzyl ester bisulfite adduct

Guidance literature:: N-cyclohexylmethyl-(2,2-diethoxyethyl)carbamic acid benzyl ester; With hydrogenchloride; In water; acetonitrile; at 30 ℃; for 7h; Inert atmosphere;

With sodium hydrogensulfite; In ethyl acetate; Inert atmosphere;
DOI:10.1021/acsmedchemlett.9b00406

Reference yield:

: 2043-61-0
cyclohexanecarbaldehyde

: 949903-23-5
N-cyclohexylmethyl-(2-oxoethyl)carbamic acid benzyl ester bisulfite adduct

Guidance literature:: Multi-step reaction with 2 steps

1.1: 2-methyltetrahydrofuran / 0.5 h / 20 °C / Inert atmosphere

1.2: 2 h / 0 °C / Inert atmosphere

1.3: 3.5 h / 0 - 20 °C / Inert atmosphere

2.1: hydrogenchloride / water; acetonitrile / 7 h / 30 °C / Inert atmosphere

2.2: Inert atmosphere

With hydrogenchloride; In 2-methyltetrahydrofuran; water; acetonitrile;
DOI:10.1021/acsmedchemlett.9b00406