3H-Imidazo[1,2-a]indol-3-one, 1,2,9,9a-tetrahydro-9-hydroxy-2,9-dimethyl-, (2S,9S,9aR)- (9CI)

Base Information

Chemical Name:3H-Imidazo[1,2-a]indol-3-one, 1,2,9,9a-tetrahydro-9-hydroxy-2,9-dimethyl-, (2S,9S,9aR)- (9CI)
CAS No.:496961-88-7
Molecular Formula:C₁₂H₁₄N₂O₂
Molecular Weight:218.255
Hs Code.:
Mol file:496961-88-7.mol

Synonyms:3H-Imidazo[1,2-a]indol-3-one, 1,2,9,9a-tetrahydro-9-hydroxy-2,9-dimethyl-, (2S,9S,9aR)- (9CI)

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Chemical Property of 3H-Imidazo[1,2-a]indol-3-one, 1,2,9,9a-tetrahydro-9-hydroxy-2,9-dimethyl-, (2S,9S,9aR)- (9CI)

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Technology Process of 3H-Imidazo[1,2-a]indol-3-one, 1,2,9,9a-tetrahydro-9-hydroxy-2,9-dimethyl-, (2S,9S,9aR)- (9CI)

There total 26 articles about 3H-Imidazo[1,2-a]indol-3-one, 1,2,9,9a-tetrahydro-9-hydroxy-2,9-dimethyl-, (2S,9S,9aR)- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: (2S,9R,9aS)-2,9-Dimethyl-9-triethylsilanyloxy-1,2,9,9a-tetrahydro-imidazo[1,2-a]indol-3-one

: 496961-89-8,496961-88-7
(2S,9R,9aS)-9-hydroxy-2,9-dimethyl-9,9a-dihydro-1H-imidazo[1,2-a]indol-3(2H)-one

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 0 ℃; for 0.25h;
DOI:10.1021/jo0264980

Reference yield: 85.0%

: (2S,9S,9aR)-2,9-Dimethyl-9-triethylsilanyloxy-1,2,9,9a-tetrahydro-imidazo[1,2-a]indol-3-one

: 496961-88-7
(2S,9S,9aR)-9-Hydroxy-2,9-dimethyl-1,2,9,9a-tetrahydro-imidazo[1,2-a]indol-3-one

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 0 ℃; for 0.25h;
DOI:10.1021/jo0264980

Reference yield: 45.0%

: 496961-87-6
(2S,9R)-2,9-Dimethyl-9-triethylsilanyloxy-2,9-dihydro-imidazo[1,2-a]indol-3-one

: 496961-89-8,496961-88-7
(2S,9R,9aS)-9-hydroxy-2,9-dimethyl-9,9a-dihydro-1H-imidazo[1,2-a]indol-3(2H)-one

: 496961-88-7
(2S,9S,9aR)-9-Hydroxy-2,9-dimethyl-1,2,9,9a-tetrahydro-imidazo[1,2-a]indol-3-one

Guidance literature:: (2S,9R)-2,9-Dimethyl-9-triethylsilanyloxy-2,9-dihydro-imidazo[1,2-a]indol-3-one; With hydrogen; platinum(IV) oxide; for 2h; under 760 Torr;

With tetrabutyl ammonium fluoride;
DOI:10.1021/jo0264980