Bis(1-methylethyl)aminodiethylborane

Base Information

• Chemical Name: Bis(1-methylethyl)aminodiethylborane
• CAS No.: 74663-92-6
• Molecular Formula: C₁₀H₂₄BN
• Molecular Weight: 169.118
• Hs Code.: 2931900090
• Mol file: 74663-92-6.mol

Synonyms:Bis(1-methylethyl)aminodiethylborane

Chemical Property of Bis(1-methylethyl)aminodiethylborane

Chemical Property:

• PSA: 3.24000
• LogP: 3.13650

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Bis(1-methylethyl)aminodiethylborane

There total 6 articles about Bis(1-methylethyl)aminodiethylborane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 48.0%

triethyl borane (97-94-9) + B{N(i-C3H7)2}3 (13006-02-5) → (C2H5)2BN(i-C3H7)2 (74663-92-6)

Guidance literature:

triethylaluminum; heating;

Reference yield:

B{N(i-C3H7)2}3 (13006-02-5) → (C2H5)2BN(i-C3H7)2 (74663-92-6)

Guidance literature:

With triethyl borane; triethylamine borane; 100°C, 5 h (N2);

Reference yield:

triethyl borane (97-94-9) + (trimethylsilyl)carbene (122048-59-3,115797-19-8) → (C2H5)2BN(i-C3H7)2 (74663-92-6) + (((CH3)2CH)2N)PC(Si(CH3)3)(C2H5)

Guidance literature:

In toluene; Irradiation (UV/VIS); -80°C, few min; (31)P-NMR monitoring;

DOI:10.1039/c39930001354

upstream raw materials:

triethyl borane

B{N(i-C₃H₇)2}3

(trimethylsilyl)carbene

bis(diethylboryl)amine

Refernces