2H-1,3-Oxazine-4-carboxylicacid,tetrahydro-2-oxo-,methylester,(S)-(9CI)

Base Information

Chemical Name:2H-1,3-Oxazine-4-carboxylicacid,tetrahydro-2-oxo-,methylester,(S)-(9CI)
CAS No.:124754-46-7
Molecular Formula:C6H9NO4
Molecular Weight:159.142
Hs Code.:
Mol file:124754-46-7.mol

Synonyms:2H-1,3-Oxazine-4-carboxylicacid,tetrahydro-2-oxo-,methylester,(S)-(9CI)

Suppliers and Price of 2H-1,3-Oxazine-4-carboxylicacid,tetrahydro-2-oxo-,methylester,(S)-(9CI)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 2 raw suppliers

Chemical Property of 2H-1,3-Oxazine-4-carboxylicacid,tetrahydro-2-oxo-,methylester,(S)-(9CI)

Chemical Property:

PSA：64.63000
LogP:-0.01330

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 2H-1,3-Oxazine-4-carboxylicacid,tetrahydro-2-oxo-,methylester,(S)-(9CI)

There total 3 articles about 2H-1,3-Oxazine-4-carboxylicacid,tetrahydro-2-oxo-,methylester,(S)-(9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 17.0%

: (S)-2-[(benzyloxycarbonyl)amino]-4-iodobutyric acid methyl ester

: 4886-44-6
(hydroxymethyl)-H-phosphinic acid

: P-benzylhydroxymethylphosphinic acid

: 868523-18-6
methyl (2S)-2-benzyloxycarbonylamino-4-(hydroxymethyl(hydroxy)phosphino)butyrate

: 124754-46-7
4-(methoxycarbonyl)tetrahydro-1,3-oxazin-2-one

Guidance literature:: (hydroxymethyl)-H-phosphinic acid; With 1,1,1,3,3,3-hexamethyl-disilazane; at 90 ℃; for 2h;

(S)-2-[(benzyloxycarbonyl)amino]-4-iodobutyric acid methyl ester; at 90 ℃; for 6h;
DOI:10.1021/jm050474e

Reference yield: 1.2%

: (S)-2-[(benzyloxycarbonyl)amino]-4-iodobutyric acid methyl ester

: 131066-43-8
N-benzyloxycarbonylaminomethyl-H-phosphinic acid

: aminomethyl(P-hydroxymethyl)phosphinic acid

: methyl (2S)-2-amino-4[(aminomethyl)(hydroxy)phosphinyl]butyrate

: benzyl-(benzyloxycarbonylamino-methyl)-phosphinic acid

: 124754-46-7
4-(methoxycarbonyl)tetrahydro-1,3-oxazin-2-one

Guidance literature:: N-benzyloxycarbonylaminomethyl-H-phosphinic acid; With 1,1,1,3,3,3-hexamethyl-disilazane; at 90 ℃; for 1h;

(S)-2-[(benzyloxycarbonyl)amino]-4-iodobutyric acid methyl ester; at 80 ℃; for 6h;

With hydrogen; palladium on activated charcoal; In methanol; for 2h;
DOI:10.1021/jm050474e

Reference yield:

: (S)-2-[(benzyloxycarbonyl)amino]-4-iodobutyric acid methyl ester

: 131066-43-8
N-benzyloxycarbonylaminomethyl-H-phosphinic acid

: N-benzyloxycarbonylaminomethyl(hydroxymethyl)phosphinic acid

: benzyl-(benzyloxycarbonylamino-methyl)-phosphinic acid

: (S)-2-Benzyloxycarbonylamino-4-[(benzyloxycarbonylamino-methyl)-hydroxy-phosphinoyl]-butyric acid methyl ester

: 124754-46-7
4-(methoxycarbonyl)tetrahydro-1,3-oxazin-2-one

Guidance literature:: N-benzyloxycarbonylaminomethyl-H-phosphinic acid; With 1,1,1,3,3,3-hexamethyl-disilazane; at 90 ℃; for 1h;

(S)-2-[(benzyloxycarbonyl)amino]-4-iodobutyric acid methyl ester; at 80 ℃; for 6h;
DOI:10.1021/jm050474e