(r)-tert-butyl 5-methyl-1,2,3-oxathiazolidine-3-carboxylate 2,2-dioxide

Base Information

Chemical Name:(r)-tert-butyl 5-methyl-1,2,3-oxathiazolidine-3-carboxylate 2,2-dioxide
CAS No.:863453-61-6
Molecular Formula:C₈H₁₅NO₅S
Molecular Weight:237.277
Hs Code.:

Synonyms:(r)-tert-butyl 5-methyl-1,2,3-oxathiazolidine-3-carboxylate 2,2-dioxide;tert-butyl (5R)-5-methyl-2,2-dioxo-1,2λ6,3-oxathiazolidine-3-carboxylate

Suppliers and Price of (r)-tert-butyl 5-methyl-1,2,3-oxathiazolidine-3-carboxylate 2,2-dioxide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Total 17 raw suppliers

Chemical Property of (r)-tert-butyl 5-methyl-1,2,3-oxathiazolidine-3-carboxylate 2,2-dioxide

Chemical Property:

Purity/Quality:: 99%, ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

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Technology Process of (r)-tert-butyl 5-methyl-1,2,3-oxathiazolidine-3-carboxylate 2,2-dioxide

There total 5 articles about (r)-tert-butyl 5-methyl-1,2,3-oxathiazolidine-3-carboxylate 2,2-dioxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 863453-61-6
tert-butyl (5R)-5-methyl-2,2-dioxo-1,2λ⁶,3-oxathiazolidine-3-carboxylate

Guidance literature:: With sulfuryl dichloride; N-ethyl-N,N-diisopropylamine; In 1,2-dichloro-ethane; at -10 ℃; for 1h; Inert atmosphere;

Reference yield: 60.6%

: 5-methyl-2-oxo-2λ⁴-[1,2,3]oxathiazolidine-3-carboxylic acid tert-butyl ester

: 863453-61-6
tert-butyl (5R)-5-methyl-2,2-dioxo-1,2λ⁶,3-oxathiazolidine-3-carboxylate

Guidance literature:: With ruthenium (III) chloride; sodium (meta)periodate; In water monomer; acetonitrile; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1016/j.bmcl.2022.128646

Reference yield:

: 119768-44-4
tert-butyl [(2R)-2-hydroxypropyl]carbamate

: 863453-61-6
tert-butyl (5R)-5-methyl-2,2-dioxo-1,2λ⁶,3-oxathiazolidine-3-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: SOCl₂; imidazole / CH₂Cl₂ / -50 °C

2: NaIO₄; RuO₂ / ethyl acetate

With 1H-imidazole; ruthenium(IV) oxide; sodium (meta)periodate; thionyl chloride; In dichloromethane; ethyl acetate;
DOI:10.1016/j.bmcl.2005.05.074