3-nitro-N-acrylphenylamine

Base Information

• Chemical Name: 3-nitro-N-acrylphenylamine
• CAS No.: 17090-15-2
• Molecular Formula: C₉H₈N₂O₃
• Molecular Weight: 192.174
• Mol file: 17090-15-2.mol

Synonyms:3-nitro-N-acrylphenylamine

Chemical Property of 3-nitro-N-acrylphenylamine

Chemical Property:

• PSA: 0.00000
• LogP: 0.00000
• Storage Temp.: under inert gas (nitrogen or Argon) at 2-8°C

Purity/Quality:

97% ^*data from raw suppliers

N-(3-Nitrophenyl)Acrylamide ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 3-nitro-N-acrylphenylamine

There total 3 articles about 3-nitro-N-acrylphenylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

acryloyl chloride (814-68-6,25189-84-8) + 3-nitro-aniline (99-09-2) → Ν-(3-nitrophenyl)acrylamide (17090-15-2)

Guidance literature:

With sodium hydrogencarbonate; In acetonitrile; at 20 ℃; for 0.5h;

DOI:10.1016/j.bmc.2016.09.001 DOI:10.1016/j.ejmech.2016.11.047 DOI:10.1016/j.bmc.2018.07.007

Reference yield: 62.3%

→ Ν-(3-nitrophenyl)acrylamide (17090-15-2)

Guidance literature:

With N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; at 20 ℃; for 1h;

Reference yield:

→ N-(4-nitrophenyl) acrylamide (7766-38-3) + Ν-(3-nitrophenyl)acrylamide (17090-15-2)

Guidance literature:

upstream raw materials:

acryloyl chloride

3-nitro-aniline

Downstream raw materials:

N-(3-Nitro-phenyl)-3-(4-pyridin-2-yl-piperazin-1-yl)-propionamide

1,4,5,6,7,7-Hexabromo-bicyclo[2.2.1]hept-5-ene-2-carboxylic acid (3-nitro-phenyl)-amide

N-(3-(N-(1-(2-chlorophenyl)-2-(3,3-difluorocyclobutylamino)-2-oxoethyl)-2-(pyridin-3-yl)acetamido)phenyl)acrylamide

Ν-(3-aminophenyl)prop-2-enamide