4-AcetaMido-N-(2-nitrophenyl)benzenesulfonaMide, 97%

Base Information

• Chemical Name: 4-AcetaMido-N-(2-nitrophenyl)benzenesulfonaMide, 97%
• CAS No.: 7461-20-3
• Molecular Formula: C14H13N3O5S
• Molecular Weight: 335.34
• Mol file: 7461-20-3.mol

Synonyms:N-Acetyl-sulfanilsaeure-(2-nitro-anilid);N-acetyl-sulfanilic acid-(2-nitro-anilide);N-{4-[(2-nitrophenyl)sulfamoyl]phenyl}acetamide;GNF-Pf-424;N4-Acetyl-N1-(o-nitro-phenyl)-sulfanilamid;N4-Acetyl-N1-(2-nitrophenyl)-sulfanilamid;Essigsaeure-[4-(2-nitro-phenylsulfamoyl)-anilid];

Chemical Property of 4-AcetaMido-N-(2-nitrophenyl)benzenesulfonaMide, 97%

Chemical Property:

• Boiling Point: °Cat760mmHg
• Flash Point: °C
• PSA: 129.47000
• Density: 1.5g/cm³
• LogP: 4.10400

Purity/Quality:

99% ^*data from raw suppliers

N-(4-{[(2-nitrophenyl)amino]sulfonyl}phenyl)acetamide ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 4-AcetaMido-N-(2-nitrophenyl)benzenesulfonaMide, 97%

There total 2 articles about 4-AcetaMido-N-(2-nitrophenyl)benzenesulfonaMide, 97% which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-nitro-aniline (88-74-4) + p-acetylaminobenzenesulfonyl chloride (121-60-8) → N-acetyl-sulfanilic acid-(2-nitro-anilide) (7461-20-3)

Guidance literature:

With N,N-dimethyl-aniline;

DOI:10.1021/ja01274a009

Reference yield:

Acetanilid (103-84-4) → N-acetyl-sulfanilic acid-(2-nitro-anilide) (7461-20-3)

Guidance literature:

Multi-step reaction with 2 steps

1: chlorosulfonic acid / 0.5 h / 60 °C

2: pyridine / 4 h / 0 - 20 °C

With pyridine; chlorosulfonic acid;

DOI:10.1016/j.ejmech.2020.112890

Reference yield:

N-acetyl-sulfanilic acid-(2-nitro-anilide) (7461-20-3) → o-nitro-N1-phenylsulfanylamide (19837-88-8)

Guidance literature:

With hydrogenchloride; ethanol;

upstream raw materials:

2-nitro-aniline

p-acetylaminobenzenesulfonyl chloride

Acetanilid

Downstream raw materials:

o-nitro-N¹-phenylsulfanylamide

N-acetyl-sulfanilic acid-(2-amino-anilide)

1-(4-acetylamino-benzenesulfonyl)-1H-benzotriazole

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