3-ETHOXYTHIOCARBONYLSULFAMYL-PHENYL ACETIC ACID

Base Information

• Chemical Name: 3-ETHOXYTHIOCARBONYLSULFAMYL-PHENYL ACETIC ACID
• CAS No.: 887354-92-9
• Molecular Formula: C11H13NO5S2
• Molecular Weight: 256.346
• Mol file: 887354-92-9.mol

Synonyms:3-ETHOXYTHIOCARBONYLSULFAMYL-PHENYL ACETIC ACID;3-[(EthoxythioxoMethyl)thio]benzeneacetic Acid

Chemical Property of 3-ETHOXYTHIOCARBONYLSULFAMYL-PHENYL ACETIC ACID

Chemical Property:

• Solubility.: Chloroform, Ethyl Acetate

Purity/Quality:

85.0-99.8% ^*data from raw suppliers

3-EthoxythiocarbonylsulfamylphenylAceticAcid ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Uses: 3-EthoxythiocarbonylsulfaMylphenyl Acetic Acid is a useful synthetic intermediate for the preparation of novel antiinflammatory agents.

Technology Process of 3-ETHOXYTHIOCARBONYLSULFAMYL-PHENYL ACETIC ACID

There total 2 articles about 3-ETHOXYTHIOCARBONYLSULFAMYL-PHENYL ACETIC ACID which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3-amino phenylacetic acid (14338-36-4) + potassium ethyl xanthogenate (140-89-6) → 2-(3-((ethoxycarbonothioyl)thio)phenyl)acetic acid (887354-92-9)

Guidance literature:

With hydrogenchloride; sodium nitrite; Multistep reaction; 1.) H₂O, 2.) 60 deg C, 90 deg C, 0.5 h;

DOI:10.1021/ja00369a041

Reference yield:

3-nitro-benzeneacetic acid (1877-73-2) → 2-(3-((ethoxycarbonothioyl)thio)phenyl)acetic acid (887354-92-9)

Guidance literature:

Multi-step reaction with 2 steps

1: 70 percent / FeSO₄-7H₂O, NH₄OH / H₂O / 0.17 h / Heating; pH 10

2: 1.) sodium nitrite, HCl / 1.) H₂O, 2.) 60 deg C, 90 deg C, 0.5 h

With hydrogenchloride; ammonium hydroxide; iron(II) sulfate; sodium nitrite; In water;

DOI:10.1021/ja00369a041

Reference yield:

2-(3-((ethoxycarbonothioyl)thio)phenyl)acetic acid (887354-92-9) → 2-(3-mercaptophenyl)acetic acid (63271-86-3)

Guidance literature:

With sodium hydroxide; In water; for 5h; Heating;

DOI:10.1021/ja00369a041

upstream raw materials:

3-amino phenylacetic acid

potassium ethyl xanthogenate

3-nitro-benzeneacetic acid

Downstream raw materials:

2-(3-mercaptophenyl)acetic acid

3,3'-dithiobis(phenylacetic acid)

3,3'-dithiobis(phenylacetyl chloride)

ethyl 2-(3-(ethylthio)phenyl)acetate

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