1-fluoro-4-iodo-2-Methoxybenzene

Base Information

• Chemical Name: 1-fluoro-4-iodo-2-Methoxybenzene
• CAS No.: 773855-64-4
• Molecular Formula: C7H6FIO
• Molecular Weight: 252.027
• Hs Code.: 2909309090
• Mol file: 773855-64-4.mol

Synonyms:1-fluoro-4-iodo-2-Methoxybenzene

Chemical Property of 1-fluoro-4-iodo-2-Methoxybenzene

Chemical Property:

• Vapor Pressure: 0.036mmHg at 25°C
• Boiling Point: 249.5°C at 760 mmHg
• Flash Point: 104.7°C
• PSA: 9.23000
• Density: 1.803g/cm³
• LogP: 2.43890
• Storage Temp.: 2-8°C(protect from light)

Purity/Quality:

97% ^*data from raw suppliers

1-Fluoro-4-iodo-2-methoxybenzene ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1-fluoro-4-iodo-2-Methoxybenzene

There total 1 articles about 1-fluoro-4-iodo-2-Methoxybenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

4-fluoro-3-methoxyaniline (64465-53-8) → 1-fluoro-4-iodo-2-methoxybenzene (773855-64-4)

Guidance literature:

4-fluoro-3-methoxyaniline; With sulfuric acid; sodium nitrite; In water; at 0 ℃; for 1h; Ice/methanol bath;

With potassium iodide; In water; at 20 ℃; for 18h;

Reference yield: 95.0%

1-fluoro-4-iodo-2-methoxybenzene (773855-64-4) + potassium thioacetate (10387-40-3) → (4-fluoro-3-methoxyphenyl)ethanethioate

Guidance literature:

With copper(l) iodide; 1,10-Phenanthroline; In toluene; at 100 ℃; for 16h; Inert atmosphere;

Reference yield: 94.0%

3-Chloro-5-ethynylpyridine (329202-22-4) + 1-fluoro-4-iodo-2-methoxybenzene (773855-64-4) → 3-chloro-5-(4-fluoro-3-methoxyphenylethynyl)-pyridine (866687-10-7)

Guidance literature:

With triethylamine; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; at 20 ℃; for 18h;

upstream raw materials:

4-fluoro-3-methoxyaniline

Downstream raw materials:

3-chloro-5-(4-fluoro-3-methoxyphenylethynyl)-pyridine

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