5-Fluoro-2-Methoxy-pyridin-3-ylaMine

Base Information

• Chemical Name: 5-Fluoro-2-Methoxy-pyridin-3-ylaMine
• CAS No.: 1211541-93-3
• Molecular Formula: C₆H₇FN₂O
• Molecular Weight: 142.133
• Hs Code.: 2933599590
• Mol file: 1211541-93-3.mol

Synonyms:5-Fluoro-2-Methoxy-pyridin-3-ylaMine;5-Fluoro-2-Methoxypyridin-3-aMine

Chemical Property of 5-Fluoro-2-Methoxy-pyridin-3-ylaMine

Chemical Property:

• PSA: 48.14000
• LogP: 1.39270
• Storage Temp.: Keep in dark place,Inert atmosphere,Room temperature

Purity/Quality:

97% ^*data from raw suppliers

5-Fluoro-2-methoxypyridin-3-amine 95+% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 5-Fluoro-2-Methoxy-pyridin-3-ylaMine

There total 9 articles about 5-Fluoro-2-Methoxy-pyridin-3-ylaMine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

5-fluoro-2-methoxy-3-nitropyridine (1211534-27-8) → 5-fluoro-2-methoxy-pyridin-3-amine (1211541-93-3)

Guidance literature:

With hydrogen; palladium 10% on activated carbon; In ethanol; at 20 ℃; for 5h;

Reference yield: 30.0%

6-chloro-5-fluoro-2-methoxy-pyridin-3-amine → 5-fluoro-2-methoxy-pyridin-3-amine (1211541-93-3)

Guidance literature:

6-chloro-5-fluoro-2-methoxy-pyridin-3-amine; With palladium on carbon; In methanol; for 0.0833333h; Inert atmosphere;

With hydrogen; In methanol; at 20 ℃; for 16h; Inert atmosphere;

Reference yield:

5-fluoro-2-hydroxy-3-nitropyridine (136888-20-5) → 5-fluoro-2-methoxy-pyridin-3-amine (1211541-93-3)

Guidance literature:

Multi-step reaction with 2 steps

1: silver carbonate / chloroform / 20 °C

2: hydrogen / palladium 10% on activated carbon / ethanol / 5 h / 20 °C

With hydrogen; silver carbonate; palladium 10% on activated carbon; In ethanol; chloroform;

upstream raw materials:

5-fluoropyridin-2-ol

5-fluoro-2-hydroxy-3-nitropyridine

5-fluoro-2-methoxy-3-nitropyridine

2,5-difluoropyridine

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