n'-Cycloheptylidene-4-methylbenzenesulfonohydrazide

Base Information

Chemical Name:n'-Cycloheptylidene-4-methylbenzenesulfonohydrazide
CAS No.:56382-69-5
Molecular Formula:C14H20N2O2S
Molecular Weight:280.391
Hs Code.:
NSC Number:126972
DSSTox Substance ID:DTXSID20298922
Nikkaji Number:J2.998.447F

Synonyms:n'-cycloheptylidene-4-methylbenzenesulfonohydrazide;56382-69-5;NSC126972;SCHEMBL20556203;DTXSID20298922;AKOS003867344;NSC-126972

Suppliers and Price of n'-Cycloheptylidene-4-methylbenzenesulfonohydrazide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of n'-Cycloheptylidene-4-methylbenzenesulfonohydrazide

Chemical Property:

Boiling Point:429°Cat760mmHg
Flash Point:213.3°C
Density:1.21g/cm³
XLogP3:3
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:3
Exact Mass:280.12454906
Heavy Atom Count:19
Complexity:394

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CC=C(C=C1)S(=O)(=O)NN=C2CCCCCC2

Technology Process of n'-Cycloheptylidene-4-methylbenzenesulfonohydrazide

There total 5 articles about n'-Cycloheptylidene-4-methylbenzenesulfonohydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 1576-35-8
toluene-4-sulfonic acid hydrazide

: 502-42-1
cycloheptanone

: 56382-69-5
cycloheptanone p-tolylsulfonylhydrazone

Guidance literature:: In methanol; at 20 ℃; Schlenk technique;
DOI:10.1021/jo501624t

Reference yield: 85.0%

: 85814-69-3
C₁₄H₁₉N₃O₄S

: 56382-69-5
cycloheptanone p-tolylsulfonylhydrazone

Guidance literature:: With lithium aluminium tetrahydride; In tetrahydrofuran; at 0 ℃; for 2h;
DOI:10.1055/s-1983-30254

Reference yield:

: 13154-27-3
2-nitrocycloheptanone

: 56382-69-5
cycloheptanone p-tolylsulfonylhydrazone

Guidance literature:: Multi-step reaction with 2 steps

1: 93 percent / sulfuric acid / methanol / 10 h / Ambient temperature

2: 85 percent / LiAlH₄ / tetrahydrofuran / 2 h / 0 °C

With lithium aluminium tetrahydride; sulfuric acid; In tetrahydrofuran; methanol;
DOI:10.1055/s-1983-30254