Technology Process of 3-O-[2,3,4,6-Tetrakis-O-(phenylmethyl)-alpha-D-glucopyranosyl]-beta-D-glucopyranose tetraacetate
There total 6 articles about 3-O-[2,3,4,6-Tetrakis-O-(phenylmethyl)-alpha-D-glucopyranosyl]-beta-D-glucopyranose tetraacetate which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
2,4,6-trimethyl-pyridine; silver perchlorate;
In
1,2-dimethoxyethane; diethyl ether;
for 3h;
Ambient temperature;
DOI:10.1016/0008-6215(92)84098-D
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 80 percent / pyridine / 0.33 h / Heating
2: 96 percent / H2, 10percent Pd/C, acetic acid / 760 Torr / Ambient temperature
3: 61 percent / AgClO4, 2,4,6-trimethylpyridine / 1,2-dimethoxy-ethane; diethyl ether / 3 h / Ambient temperature
With
pyridine; 2,4,6-trimethyl-pyridine; palladium on activated charcoal; hydrogen; silver perchlorate; acetic acid;
In
1,2-dimethoxyethane; diethyl ether;
DOI:10.1016/0008-6215(92)84098-D
- Guidance literature:
-
Multi-step reaction with 4 steps
1: Amberlite IR-120 (H(1+)) / H2O / 5 h / 80 °C
2: 80 percent / pyridine / 0.33 h / Heating
3: 96 percent / H2, 10percent Pd/C, acetic acid / 760 Torr / Ambient temperature
4: 61 percent / AgClO4, 2,4,6-trimethylpyridine / 1,2-dimethoxy-ethane; diethyl ether / 3 h / Ambient temperature
With
pyridine; 2,4,6-trimethyl-pyridine; palladium on activated charcoal; Amberlite IR-120 (H(1+)); hydrogen; silver perchlorate; acetic acid;
In
1,2-dimethoxyethane; diethyl ether; water;
DOI:10.1016/0008-6215(92)84098-D
