3-O-[2,3,4,6-Tetrakis-O-(phenylmethyl)-alpha-D-glucopyranosyl]-beta-D-glucopyranose tetraacetate

Base Information

Chemical Name:3-O-[2,3,4,6-Tetrakis-O-(phenylmethyl)-alpha-D-glucopyranosyl]-beta-D-glucopyranose tetraacetate
CAS No.:140420-82-2
Molecular Formula:C₄₈H₅₄O₁₅
Molecular Weight:870.948
Hs Code.:

Synonyms:3-O-[2,3,4,6-Tetrakis-O-(phenylmethyl)-alpha-D-glucopyranosyl]-beta-D-glucopyranose tetraacetate

Suppliers and Price of 3-O-[2,3,4,6-Tetrakis-O-(phenylmethyl)-alpha-D-glucopyranosyl]-beta-D-glucopyranose tetraacetate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 2 raw suppliers

Chemical Property of 3-O-[2,3,4,6-Tetrakis-O-(phenylmethyl)-alpha-D-glucopyranosyl]-beta-D-glucopyranose tetraacetate

Chemical Property:

Purity/Quality:: 95% ^*data from raw suppliers

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Technology Process of 3-O-[2,3,4,6-Tetrakis-O-(phenylmethyl)-alpha-D-glucopyranosyl]-beta-D-glucopyranose tetraacetate

There total 6 articles about 3-O-[2,3,4,6-Tetrakis-O-(phenylmethyl)-alpha-D-glucopyranosyl]-beta-D-glucopyranose tetraacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

: 25320-59-6
tetra-O-benzyl glucopyranosyl chloride

: 27086-14-2
1,2,4,6-tetra-O-acetyl-β-D-glucopyranose

: 140420-82-2
O-(2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl)-(1->3)-1,2,4,6-tetra-O-acetyl-β-D-glucopyranose

Guidance literature:: With 2,4,6-trimethyl-pyridine; silver perchlorate; In 1,2-dimethoxyethane; diethyl ether; for 3h; Ambient temperature;
DOI:10.1016/0008-6215(92)84098-D

Reference yield:

: 65877-63-6,97590-76-6,99396-09-5,5531-09-9
3-O-benzyl-D-glucopyranose

: 140420-82-2
O-(2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl)-(1->3)-1,2,4,6-tetra-O-acetyl-β-D-glucopyranose

Guidance literature:: Multi-step reaction with 3 steps

1: 80 percent / pyridine / 0.33 h / Heating

2: 96 percent / H₂, 10percent Pd/C, acetic acid / 760 Torr / Ambient temperature

3: 61 percent / AgClO₄, 2,4,6-trimethylpyridine / 1,2-dimethoxy-ethane; diethyl ether / 3 h / Ambient temperature

With pyridine; 2,4,6-trimethyl-pyridine; palladium on activated charcoal; hydrogen; silver perchlorate; acetic acid; In 1,2-dimethoxyethane; diethyl ether;
DOI:10.1016/0008-6215(92)84098-D

Reference yield:

: 18685-18-2
3-O-benzyl-1,2-5,6-O-diisopropylidene-α-D-glucofuranose

: 140420-82-2
O-(2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl)-(1->3)-1,2,4,6-tetra-O-acetyl-β-D-glucopyranose

Guidance literature:: Multi-step reaction with 4 steps

1: Amberlite IR-120 (H⁽¹⁺⁾) / H₂O / 5 h / 80 °C

2: 80 percent / pyridine / 0.33 h / Heating

3: 96 percent / H₂, 10percent Pd/C, acetic acid / 760 Torr / Ambient temperature

4: 61 percent / AgClO₄, 2,4,6-trimethylpyridine / 1,2-dimethoxy-ethane; diethyl ether / 3 h / Ambient temperature

With pyridine; 2,4,6-trimethyl-pyridine; palladium on activated charcoal; Amberlite IR-120 (H⁽¹⁺⁾); hydrogen; silver perchlorate; acetic acid; In 1,2-dimethoxyethane; diethyl ether; water;
DOI:10.1016/0008-6215(92)84098-D