(S)-tert-butyl 3-(piperazin-1-yl) pyrrolidine-1-carboxylate

Base Information

• Chemical Name: (S)-tert-butyl 3-(piperazin-1-yl) pyrrolidine-1-carboxylate
• CAS No.: 1010446-31-7
• Molecular Formula: C₁₃H₂₅N₃O₂
• Molecular Weight: 255.36
• Hs Code.: 2933990090
• Mol file: 1010446-31-7.mol

Synonyms:(S)-tert-butyl 3-(piperazin-1-yl) pyrrolidine-1-carboxylate;(3S)-3-(1-Piperazinyl)-1-pyrrolidinecarboxylic acid tert-butyl ester

Chemical Property of (S)-tert-butyl 3-(piperazin-1-yl) pyrrolidine-1-carboxylate

Chemical Property:

• PSA: 44.81000
• Density: 1.090
• LogP: 1.10560
• Storage Temp.: under inert gas (nitrogen or Argon) at 2–8 °C

Purity/Quality:

97% ^*data from raw suppliers

tert-butyl(S)-3-(piperazin-1-yl)pyrrolidine-1-carboxylate 97% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of (S)-tert-butyl 3-(piperazin-1-yl) pyrrolidine-1-carboxylate

There total 2 articles about (S)-tert-butyl 3-(piperazin-1-yl) pyrrolidine-1-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

tert-butyl (S)-3-(4-benzylpiperazin-1-yl)pyrrolidine-1-carboxylate (717927-56-5) → (S)-3-piperazin-1-yl-pyrrolidine-1-carboxylic acid tert-butyl ester (1010446-31-7)

Guidance literature:

With hydrogen; acetic acid; palladium 10% on activated carbon; In ethanol; for 18h; under 760.051 Torr;

Reference yield:

→ (S)-3-piperazin-1-yl-pyrrolidine-1-carboxylic acid tert-butyl ester (1010446-31-7)

Guidance literature:

Reference yield:

(S)-3-piperazin-1-yl-pyrrolidine-1-carboxylic acid tert-butyl ester (1010446-31-7) + C21H15Cl2F6NO2 (717927-55-4) → C29H32Cl2F6N4O

Guidance literature:

Multi-step reaction with 2 steps

1: thiophene; titanium, tetrakis (2-propanolato); hydrogen / 5 % platinum on carbon / methanol / 50 °C

2: hydrogenchloride / isopropyl alcohol / 2 h / Heating / reflux

With thiophene; hydrogenchloride; titanium, tetrakis (2-propanolato); hydrogen; 5 % platinum on carbon; In methanol; isopropyl alcohol;

upstream raw materials:

tert-butyl (S)-3-(4-benzylpiperazin-1-yl)pyrrolidine-1-carboxylate

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