1,2,5-Thiadiazepane 1,1-dioxide

Base Information

• Chemical Name: 1,2,5-Thiadiazepane 1,1-dioxide
• CAS No.: 410545-38-9
• Molecular Formula: C4H10N2O2S
• Molecular Weight: 150.1994
• Hs Code.: 2934100090
• Mol file: 410545-38-9.mol

Synonyms:1,2,5-Thiadiazepane 1,1-dioxide;Hexahydro-1,2,5-thiadiazepine 1,1-dioxide

Chemical Property of 1,2,5-Thiadiazepane 1,1-dioxide

Chemical Property:

• Boiling Point: 285.4±50.0℃ (760 Torr)
• Flash Point: 126.4±30.1℃
• PSA: 66.58000
• Density: 1.222±0.06 g/cm3 (20 oC 760 Torr)
• LogP: 0.24740

Purity/Quality:

97% ^*data from raw suppliers

1lambda(6),2,5-Thiadiazepane-1,1-dione 95+% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1,2,5-Thiadiazepane 1,1-dioxide

There total 2 articles about 1,2,5-Thiadiazepane 1,1-dioxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N-(2-aminoethyl)ethenesulfonamide hydrochloride (410545-37-8) → 1,2,5-thiadiazepane 1,1-dioxide (410545-38-9)

Guidance literature:

With triethylamine; In methanol; acetonitrile;

Reference yield:

5-[(2-nitrophenyl)sulfonyl]-1,2,5-thiadiazepane 1,1-dioxide → 1,2,5-thiadiazepane 1,1-dioxide (410545-38-9)

Guidance literature:

With potassium carbonate; para-thiocresol; In acetonitrile; at 50 ℃; for 21h;

Reference yield:

1,2,5-thiadiazepane 1,1-dioxide (410545-38-9) + C24H25N4O5PolS → C28H33N6O6PolS2

Guidance literature:

With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; at 20 ℃; for 3h; Not specified

upstream raw materials:

N-(2-aminoethyl)ethenesulfonamide hydrochloride

Refernces

• 1、 -. "PYRIMIDINE DERIVATIVE CONDENSED WITH NON-AROMATIC RING". Page/Page column 18. . Retrieved 2010/11/27.