N-[(9H-Fluoren-9-ylmethoxy)carbonyl]-O-(2,3,4,6-tetra-O-acetyl-beta-D-galactopyranosyl)-L-serine pentafluorophenyl ester

Base Information

Chemical Name:N-[(9H-Fluoren-9-ylmethoxy)carbonyl]-O-(2,3,4,6-tetra-O-acetyl-beta-D-galactopyranosyl)-L-serine pentafluorophenyl ester
CAS No.:243469-45-6
Molecular Formula:C38H34F5NO14
Molecular Weight:0
Hs Code.:
Mol file:243469-45-6.mol

Synonyms:N-[(9H-Fluoren-9-ylmethoxy)carbonyl]-O-(2,3,4,6-tetra-O-acetyl-beta-D-galactopyranosyl)-L-serine pentafluorophenyl ester

Suppliers and Price of N-[(9H-Fluoren-9-ylmethoxy)carbonyl]-O-(2,3,4,6-tetra-O-acetyl-beta-D-galactopyranosyl)-L-serine pentafluorophenyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of N-[(9H-Fluoren-9-ylmethoxy)carbonyl]-O-(2,3,4,6-tetra-O-acetyl-beta-D-galactopyranosyl)-L-serine pentafluorophenyl ester

Chemical Property:

Purity/Quality:: 95% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of N-[(9H-Fluoren-9-ylmethoxy)carbonyl]-O-(2,3,4,6-tetra-O-acetyl-beta-D-galactopyranosyl)-L-serine pentafluorophenyl ester

There total 1 articles about N-[(9H-Fluoren-9-ylmethoxy)carbonyl]-O-(2,3,4,6-tetra-O-acetyl-beta-D-galactopyranosyl)-L-serine pentafluorophenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 86061-05-4
N^α-(fluoren-9-ylmethoxycarbonyl)-L-serine pentafluorophenyl ester

: 4163-60-4
β-D-galactose peracetate

: 243469-45-6
N^α-(9-Fluorenylmethoxycarbonyl)-3-O-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)-L-serine pentafluorophenyl ester

Guidance literature:: With boron trifluoride diethyl etherate; In dichloromethane; at 20 ℃;
DOI:10.1016/S0040-4039(00)00611-0

Reference yield: 97.0%

: 97-69-8
(S)-acetamidoalanine

: 5241-58-7
L-Phenylalanine amide

: 243469-45-6
N^α-(9-Fluorenylmethoxycarbonyl)-3-O-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)-L-serine pentafluorophenyl ester

: 291311-51-8
Ac-Ala-Ser[β-Gal(OAc)4]-Phe-NH2

Guidance literature:: Multistep reaction;
DOI:10.1016/S0040-4039(00)00611-0

Reference yield:

: 243469-45-6
N^α-(9-Fluorenylmethoxycarbonyl)-3-O-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)-L-serine pentafluorophenyl ester

: (S)-2-[(S)-2-((S)-2-Acetylamino-propionylamino)-3-((2R,3R,4S,5R,6R)-3,4,5-trihydroxy-6-hydroxymethyl-tetrahydro-pyran-2-yloxy)-propionylamino]-3-phenyl-propionamide

Guidance literature:: Multi-step reaction with 2 steps

1: 97 percent

2: NaOMe / methanol / 5 h

With sodium methylate; In methanol; 2: Elimination;
DOI:10.1016/S0040-4039(00)00611-0