N,N-dimethyl-1,1-bis(2-trimethylsilylethoxy)methanamine

Base Information

• Chemical Name: N,N-dimethyl-1,1-bis(2-trimethylsilylethoxy)methanamine
• CAS No.: 129816-49-5
• Molecular Formula: C₁₃H₃₃NO₂Si₂
• Molecular Weight: 291.582
• European Community (EC) Number: 634-179-7
• DSSTox Substance ID: DTXSID50400450
• Mol file: 129816-49-5.mol

Synonyms:129816-49-5;N,N-dimethyl-1,1-bis(2-trimethylsilylethoxy)methanamine;N,N-DIMETHYLFORMAMIDE BIS(2-(TRIMETHYLSIL)ETHYL)ACETAL;N,N-DIMETHYLFORMAMIDE BIS[2-(TRIMETHYL- SILYL)ETHYL] ACETATE;SCHEMBL5407802;DTXSID50400450;GYFJJPXKRVCZPC-UHFFFAOYSA-N

Chemical Property of N,N-dimethyl-1,1-bis(2-trimethylsilylethoxy)methanamine

Chemical Property:

• Refractive Index: n20/D 1.436(lit.)
• Boiling Point: 125-127 °C11 mm Hg(lit.)
• Flash Point: 66 °C
• PSA: 21.70000
• Density: 0.859 g/mL at 25 °C(lit.)
• LogP: 3.54120
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 3
• Rotatable Bond Count: 9
• Exact Mass: 291.20498236
• Heavy Atom Count: 18
• Complexity: 202

Purity/Quality:

95% ^*data from raw suppliers

N,N-DIMETHYLFORMAMIDE BIS-(2-(TRIMETHYLSILYL)ETHYL)ACETAL 95.00% ^*data from reagent suppliers

Safty Information:

• Hazard Codes: T
• Statements: 45-20/21/22-36/37/38
• Safety Statements: 53-22-26-27-36/37/39-45

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CN(C)C(OCC[Si](C)(C)C)OCC[Si](C)(C)C

Technology Process of N,N-dimethyl-1,1-bis(2-trimethylsilylethoxy)methanamine

There total 1 articles about N,N-dimethyl-1,1-bis(2-trimethylsilylethoxy)methanamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

2-(Trimethylsilyl)ethanol (2916-68-9) + N,N-dimethyl-formamide dimethyl acetal (4637-24-5) → dimethylformamide bis(trimethylsilylethyl) acetal (129816-49-5)

Guidance literature:

at 20 - 120 ℃;

DOI:10.1021/jm00039a003

upstream raw materials:

2-(Trimethylsilyl)ethanol

N,N-dimethyl-formamide dimethyl acetal