Cyclopentaneethanol, 2-hydroxy--ba--(methoxymethoxy)-, (1S,2S)- (9CI)

Base Information

Chemical Name:Cyclopentaneethanol, 2-hydroxy--ba--(methoxymethoxy)-, (1S,2S)- (9CI)
CAS No.:642454-30-6
Molecular Formula:C9H18O4
Molecular Weight:190.23682
Hs Code.:
Mol file:642454-30-6.mol

Synonyms:Cyclopentaneethanol,2-hydroxy--bta--(methoxymethoxy)-,(1S,2S)-(9CI);Cyclopentaneethanol, 2-hydroxy--ba--(methoxymethoxy)-, (1S,2S)- (9CI)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Cyclopentaneethanol, 2-hydroxy--ba--(methoxymethoxy)-, (1S,2S)- (9CI)

Chemical Property:

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Technology Process of Cyclopentaneethanol, 2-hydroxy--ba--(methoxymethoxy)-, (1S,2S)- (9CI)

There total 4 articles about Cyclopentaneethanol, 2-hydroxy--ba--(methoxymethoxy)-, (1S,2S)- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: 642454-28-2
methyl [(1R,2S)-2-benzoyloxycyclopentyl](methoxymethoxy)acetate

: 642454-30-6,141521-32-6
(1S,2S)-2-[2-hydroxy-1-(methoxymethoxy)ethyl]cyclopentanol

Guidance literature:: With lithium aluminium tetrahydride; In diethyl ether; at 0 ℃; for 3.5h;
DOI:10.1271/bbb.67.1959

Reference yield:

: 642454-24-8
methyl [(1R,2S)-2-benzoyloxycyclopentyl]acetate

: 642454-30-6,141521-32-6
(1S,2S)-2-[2-hydroxy-1-(methoxymethoxy)ethyl]cyclopentanol

Guidance literature:: Multi-step reaction with 3 steps

1.1: LDA / tetrahydrofuran / 0.5 h / -75 °C

1.2: 54 percent / MoO₅*pyridine*HMPA / tetrahydrofuran / 0.33 h / -23 °C

2.1: 83 percent / (i-Pr)2NEt / CH₂Cl₂ / 18 h / 20 °C

3.1: 66 percent / LiAlH₄ / diethyl ether / 3.5 h / 0 °C

With lithium aluminium tetrahydride; N-ethyl-N,N-diisopropylamine; lithium diisopropyl amide; In tetrahydrofuran; diethyl ether; dichloromethane;
DOI:10.1271/bbb.67.1959

Reference yield:

: 642454-26-0
methyl [(1R,2S)-2-benzoyloxycyclopentyl](hydroxy)acetate

: 642454-30-6,141521-32-6
(1S,2S)-2-[2-hydroxy-1-(methoxymethoxy)ethyl]cyclopentanol

Guidance literature:: Multi-step reaction with 2 steps

1: 83 percent / (i-Pr)2NEt / CH₂Cl₂ / 18 h / 20 °C

2: 66 percent / LiAlH₄ / diethyl ether / 3.5 h / 0 °C

With lithium aluminium tetrahydride; N-ethyl-N,N-diisopropylamine; In diethyl ether; dichloromethane;
DOI:10.1271/bbb.67.1959