Technology Process of [2S,3S,(+)]-1-Bromo-2,3-pentanediol
There total 3 articles about [2S,3S,(+)]-1-Bromo-2,3-pentanediol which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 71 percent / HCl(conc.) / 1.) 5 deg C, 10 min 2.) 1 h, room temp.
2: 71 percent / Raney-Ni (W-2) / ethanol; H2O / 0.75 h / Ambient temperature
3: 1.) (C6H5)3P 2.) CBr4 / 1.) 0 deg C, pyridine 2.) room temp., 7-8h
With
hydrogenchloride; carbon tetrabromide; triphenylphosphine;
Raney-Ni (W-2);
In
ethanol; water;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 71 percent / Raney-Ni (W-2) / ethanol; H2O / 0.75 h / Ambient temperature
2: 1.) (C6H5)3P 2.) CBr4 / 1.) 0 deg C, pyridine 2.) room temp., 7-8h
With
carbon tetrabromide; triphenylphosphine;
Raney-Ni (W-2);
In
ethanol; water;
- Guidance literature:
-
With
carbon tetrabromide; triphenylphosphine;
Yield given. Multistep reaction;
1.) 0 deg C, pyridine 2.) room temp., 7-8h;
