8-Amino-4H-1,4-benzoxazin-3-one

Base Information

Chemical Name:8-Amino-4H-1,4-benzoxazin-3-one
CAS No.:1042973-67-0
Molecular Formula:C₈H₇ClN₂O₂
Molecular Weight:198.609
Hs Code.:
Mol file:1042973-67-0.mol

Synonyms:8-AMINO-2H-1,4-BENZOXAZIN-3(4H)-ONE;8-amino-2,4-dihydro-1,4-benzoxazin-3-one;8-AMINO-4H-1,4-BENZOXAZIN-3-ONE;

Suppliers and Price of 8-Amino-4H-1,4-benzoxazin-3-one

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
8-Amino-6-chloro-4H-benzo[1,4]oxazin-3-one
1g
$ 265.00

Crysdot
8-Amino-6-chloro-2H-benzo[b][1,4]oxazin-3(4H)-one 97%
5g
$ 447.00

Total 3 raw suppliers

Chemical Property of 8-Amino-4H-1,4-benzoxazin-3-one

Chemical Property:

PSA：64.35000
LogP:1.97230

Purity/Quality:

97% ^*data from raw suppliers

8-Amino-6-chloro-4H-benzo[1,4]oxazin-3-one ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 8-Amino-4H-1,4-benzoxazin-3-one

There total 3 articles about 8-Amino-4H-1,4-benzoxazin-3-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 870064-73-6
6-chloro-8-nitro-2H-benzo[b][1,4]oxazin-3(4H)-one

: 1042973-67-0
8-amino-6-chloro-3,4-dihydro-2H-benzo[1,4]oxazin-3-one

Guidance literature:: With hydrogen; palladium on activated charcoal; In tetrahydrofuran; at 35 ℃; for 4h;

Reference yield:

: C₁₀H₁₁ClN₂O₅

: 1042973-67-0
8-amino-6-chloro-3,4-dihydro-2H-benzo[1,4]oxazin-3-one

Guidance literature:: With iron; acetic acid; at 75 ℃;
DOI:10.1016/j.bmcl.2011.04.053

Reference yield:

: 6358-08-3
4-chloro-6-nitro-2-aminophenol

: 1042973-67-0
8-amino-6-chloro-3,4-dihydro-2H-benzo[1,4]oxazin-3-one

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / acetonitrile

2: iron; acetic acid / 75 °C

With iron; potassium carbonate; acetic acid; In acetonitrile;
DOI:10.1016/j.bmcl.2011.04.053