N-ETHYL-N'-[5-(4,4,5,5-TETRAMETHYL-1,3,2-DIOXABOROLAN-2-YL)-2-PYRIDINYL]-UREA

Base Information

Chemical Name:N-ETHYL-N'-[5-(4,4,5,5-TETRAMETHYL-1,3,2-DIOXABOROLAN-2-YL)-2-PYRIDINYL]-UREA
CAS No.:1031431-96-5
Molecular Formula:C14H22BN3O3
Molecular Weight:291.15378
Hs Code.:
Mol file:1031431-96-5.mol

Synonyms:N-ETHYL-N'-[5-(4,4,5,5-TETRAMETHYL-1,3,2-DIOXABOROLAN-2-YL)-2-PYRIDINYL]-UREA;1-ethyl-3-(5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)pyridin-2-yl)urea

Suppliers and Price of N-ETHYL-N'-[5-(4,4,5,5-TETRAMETHYL-1,3,2-DIOXABOROLAN-2-YL)-2-PYRIDINYL]-UREA

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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Total 5 raw suppliers

Chemical Property of N-ETHYL-N'-[5-(4,4,5,5-TETRAMETHYL-1,3,2-DIOXABOROLAN-2-YL)-2-PYRIDINYL]-UREA

Chemical Property:

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of N-ETHYL-N'-[5-(4,4,5,5-TETRAMETHYL-1,3,2-DIOXABOROLAN-2-YL)-2-PYRIDINYL]-UREA

There total 1 articles about N-ETHYL-N'-[5-(4,4,5,5-TETRAMETHYL-1,3,2-DIOXABOROLAN-2-YL)-2-PYRIDINYL]-UREA which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 827614-64-2
2-aminopyridine-5-boronic acid pinacol ester

: 109-90-0
ethyl isocyanate

: 1031431-96-5
N-ethyl-N′-[5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)pyridin-2-yl]urea

Guidance literature:: In dichloromethane; at 20 ℃;

Reference yield: 54.0%

: 1031431-96-5
N-ethyl-N′-[5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)pyridin-2-yl]urea

: 618-89-3
methyl 3-bromobenzoate

: 1031428-43-9
methyl 3-(6-{[(ethylamino)carbonyl]amino}pyridin-3-yl)benzoate

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; caesium carbonate; In 1,4-dioxane; water; at 110 ℃; for 0.5h; Microwave irradiation; Inert atmosphere;
DOI:10.1021/jm401208b

Reference yield: 43.0%

: 1031431-96-5
N-ethyl-N′-[5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)pyridin-2-yl]urea

: 619-42-1
4-methoxycarbonylphenyl bromide

: 1031428-45-1
methyl 4-(6-{[(ethylamino)carbonyl]amino}pyridin-3-yl)benzoate

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; caesium carbonate; In 1,4-dioxane; water; at 110 ℃; for 0.5h; Microwave irradiation; Inert atmosphere;
DOI:10.1021/jm401208b