5,6,7,8-Tetrahydro-3-methylisoquinoline

Base Information

• Chemical Name: 5,6,7,8-Tetrahydro-3-methylisoquinoline
• CAS No.: 37009-20-4
• Molecular Formula: C₁₀H₁₃N
• Molecular Weight: 147.22
• Mol file: 37009-20-4.mol

Synonyms:5,6,7,8-Tetrahydro-3-methylisoquinoline

Chemical Property of 5,6,7,8-Tetrahydro-3-methylisoquinoline

Chemical Property:

• Boiling Point: 93 °C (3 mmHg)
• PSA: 12.89000
• LogP: 2.26880

Purity/Quality:

99% ^*data from raw suppliers

5,6,7,8-TETRAHYDRO-3-METHYLISOQUINOLINE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 5,6,7,8-Tetrahydro-3-methylisoquinoline

There total 4 articles about 5,6,7,8-Tetrahydro-3-methylisoquinoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

1,7-Octadiyne (871-84-1) + acetonitrile (75-05-8,26809-02-9) → 3-methyl-5,6,7,8-tetrahydroquinoline (37009-20-4)

Guidance literature:

di-tert-butylphosphanylethylcyclopentadienylcobalt(I); In ethanol; at 25 ℃;

DOI:10.1039/b207978j

Reference yield: 55.0%

1,7-Octadiyne (871-84-1) + acetonitrile (75-05-8,26809-02-9) → 3-methyl-5,6,7,8-tetrahydroquinoline (37009-20-4) + 1-3.4-tetramethylen-benzol (1914-36-9)

Guidance literature:

With nickel(II) bromide dimethoxyethane; N,N,N',N'',N'''-pentamethyldiethylenetriamine; carbon dioxide; electrolysis;

DOI:10.1021/jo00061a038

Reference yield: 45.0%

1,7-Octadiyne (871-84-1) + acetonitrile (75-05-8,26809-02-9) → 3-methyl-5,6,7,8-tetrahydroquinoline (37009-20-4) + 4,6-di-5-exynyl-2-methylpyridine + 3,6-di-5-exynyl-2-methylpyridine

Guidance literature:

toluene-cobalt; at 50 ℃; for 48h;

DOI:10.1016/0022-328X(87)80138-9

upstream raw materials:

1,7-Octadiyne

acetonitrile

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