1-BroMo-3-(isopropylsulfonyl)benzene

Base Information

• Chemical Name: 1-BroMo-3-(isopropylsulfonyl)benzene
• CAS No.: 70399-01-8
• Molecular Formula: C9H11BrO2S
• Molecular Weight: 263.155
• Hs Code.: 2904909090
• Mol file: 70399-01-8.mol

Synonyms:1-BroMo-3-(isopropylsulfonyl)benzene;1-BroMo-3-(isopropanesulfonyl)benzene

Chemical Property of 1-BroMo-3-(isopropylsulfonyl)benzene

Chemical Property:

• PSA: 42.52000
• LogP: 3.71200
• Storage Temp.: Sealed in dry,Room Temperature

Purity/Quality:

97% ^*data from raw suppliers

1-Bromo-3-(isopropanesulfonyl)benzene ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1-BroMo-3-(isopropylsulfonyl)benzene

There total 3 articles about 1-BroMo-3-(isopropylsulfonyl)benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-bromo-3-isopropylsulfanylbenzene (70398-87-7) → 1-bromo-3-(isopropylsulfonyl)benzene (70399-01-8)

Guidance literature:

With dihydrogen peroxide; acetic acid;

DOI:10.1021/jo01329a011

Reference yield:

3-Bromothiophenol (6320-01-0) → 1-bromo-3-(isopropylsulfonyl)benzene (70399-01-8)

Guidance literature:

Multi-step reaction with 2 steps

1: potassium carbonate / acetone / 18 h / Inert atmosphere; Reflux

2: Oxone / water; methanol / 2 h / 0 - 20 °C

With Oxone; potassium carbonate; In methanol; water; acetone;

DOI:10.1002/cmdc.202100018

Reference yield:

3-fluorobromobenzene (1073-06-9) → 1-bromo-3-(isopropylsulfonyl)benzene (70399-01-8)

Guidance literature:

Multi-step reaction with 2 steps

2: aq. H₂O₂, AcOH

With dihydrogen peroxide; acetic acid;

DOI:10.1021/jo01329a011

upstream raw materials:

1-bromo-3-isopropylsulfanylbenzene

3-fluorobromobenzene

3-Bromothiophenol

Downstream raw materials:

2-benzyl-3-(3-(3-(isopropylsulfonyl)phenoxy)phenyl)-8-(trifluoromethyl)imidazo[1,2-a]pyridine

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