(3aR,6aS)-rel-tetrahydro-2-Methyl-Cyclopenta [c]pyrrole-1,3,5(2H)-trione (Relative stereocheMistry)

Base Information

Chemical Name:(3aR,6aS)-rel-tetrahydro-2-Methyl-Cyclopenta [c]pyrrole-1,3,5(2H)-trione (Relative stereocheMistry)
CAS No.:1175009-80-9
Molecular Formula:
Molecular Weight:167.16
Hs Code.:
Mol file:1175009-80-9.mol

Synonyms:(3aR,6aS)-rel-tetrahydro-2-Methyl-Cyclopenta [c]pyrrole-1,3,5(2H)-trione (Relative stereocheMistry)

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Chemical Property of (3aR,6aS)-rel-tetrahydro-2-Methyl-Cyclopenta [c]pyrrole-1,3,5(2H)-trione (Relative stereocheMistry)

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Technology Process of (3aR,6aS)-rel-tetrahydro-2-Methyl-Cyclopenta [c]pyrrole-1,3,5(2H)-trione (Relative stereocheMistry)

There total 4 articles about (3aR,6aS)-rel-tetrahydro-2-Methyl-Cyclopenta [c]pyrrole-1,3,5(2H)-trione (Relative stereocheMistry) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: N-methyl-4-methylene-cis-cyclopentane-1,2-dicarboximide

: 18853-53-7,1175009-80-9
1,3,5-Trioxo-2-methyl-cyclopentapyrrolidin

Guidance literature:: N-methyl-4-methylene-cis-cyclopentane-1,2-dicarboximide; With ozone; In oxygen; ethyl acetate; at -78 ℃; for 0.75h;

With 5%-palladium/activated carbon; hydrogen; In ethyl acetate; at 20 ℃; under 760.051 Torr;
DOI:10.1002/ejoc.200900273

Reference yield:

: 930-88-1
N-methylmaleimide

: 18853-53-7,1175009-80-9
1,3,5-Trioxo-2-methyl-cyclopentapyrrolidin

Guidance literature:: Multi-step reaction with 2 steps

1: 87 percent / Ni(COD)2/TOPP / tetrahydrofuran / 10 h / 120 °C

2: ozonolysis

bis(1,5-cyclooctadiene)nickel ⁽⁰⁾; In tetrahydrofuran;
DOI:10.1016/S0040-4020(01)80117-4