Zirconium tribromide

Base Information

• Chemical Name: Zirconium tribromide
• CAS No.: 24621-18-9
• Molecular Formula: Br4Zr
• Molecular Weight: 330.936
• Wikipedia: Zirconium(III)_bromide
• Wikidata: Q4096901
• Mol file: 24621-18-9.mol

Synonyms:Zirconium tribromide;Tribromozirconium;24621-18-9;Zirconium(III) bromide;Q4096901

Chemical Property of Zirconium tribromide

Chemical Property:

• PSA: 0.00000
• LogP: -11.98400
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 0
• Rotatable Bond Count: 0
• Exact Mass: 328.65766
• Heavy Atom Count: 4
• Complexity: 8

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Chemical Classes: Metals -> Metals, Inorganic Compounds
• Canonical SMILES: Br[Zr](Br)Br

Technology Process of Zirconium tribromide

There total 2 articles about Zirconium tribromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

zirconium(II)(η6-benzene)(tetrabromoaluminate)2 + zirconium(IV) bromide (13777-25-8) → zirconium (III) bromide (24621-18-9)

Guidance literature:

With aluminum tri-bromide; In benzene; byproducts: AlBr3, C6H6; (Ar); stirring at 25°C for 24 h, refluxing for 1 h, filtn., dark violet solution, transferring to a flask containing ZrBr4, stirred at 25°C for 48 h; filtn., washing with benzene, drying in vacuo, elem. anal.;

DOI:10.1039/DT9900001813

Reference yield:

zirconium(IV) bromide (13777-25-8) → zirconium (III) bromide (24621-18-9)

Guidance literature:

With Hg or Al or Ag; In acetone;

DOI:10.1021/ja01357a016

Reference yield:

zirconium (III) bromide (24621-18-9) → zirconium dibromide + zirconium(IV) bromide (13777-25-8)

Guidance literature:

In neat (no solvent); heating of 0.5 g ZrBr3 in an evacuated pyrex glass tube at 350°C, 10-15 hours or at 390°C, 6 hours; temp. should be lower than 400°C;; removal of ZrBr4;;

DOI:10.1021/ja01357a016

upstream raw materials:

zirconium(IV) bromide

Downstream raw materials:

zirconium(IV) bromide

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