N1-Isopropyl-N3-methyl-1,3-propanediamine

Base Information

• Chemical Name: N1-Isopropyl-N3-methyl-1,3-propanediamine
• CAS No.: 15937-57-2
• Molecular Formula: C₇H₁₈N₂
• Molecular Weight: 130.233
• Hs Code.: 2921290000
• Mol file: 15937-57-2.mol

Synonyms:N1-Isopropyl-N3-methyl-1,3-propanediamine

Chemical Property of N1-Isopropyl-N3-methyl-1,3-propanediamine

Chemical Property:

• Boiling Point: 175.2±8.0 °C(Predicted)
• PKA: 10.56±0.29(Predicted)
• PSA: 24.06000
• Density: 0.803±0.06 g/cm3(Predicted)
• LogP: 1.37570

Purity/Quality:

98%min ^*data from raw suppliers

N1-Isopropyl-N3-methyl-1,3-propanediamine ^*data from reagent suppliers

Safty Information:

• Hazard Codes: Xi

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of N1-Isopropyl-N3-methyl-1,3-propanediamine

There total 2 articles about N1-Isopropyl-N3-methyl-1,3-propanediamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

tert-butyl (3-(isopropylamino)propyl)(methyl)carbamate (1246248-47-4) → N1-isopropyl-N3-methylpropane-1,3-diamine (15937-57-2)

Guidance literature:

tert-butyl (3-(isopropylamino)propyl)(methyl)carbamate; With trifluoroacetic acid; In dichloromethane; for 4h;

With potassium carbonate; In dichloromethane; for 2h;

DOI:10.1039/c9cc06937b

Reference yield: 36.1%

N-Isopropylidene-N'-methyl-propane-1,3-diamine → N1-isopropyl-N3-methylpropane-1,3-diamine (15937-57-2)

Guidance literature:

With sodium tetrahydroborate; In methanol; at 20 ℃; for 3h; Inert atmosphere;

DOI:10.1002/chem.202001436

upstream raw materials:

tert-butyl (3-(isopropylamino)propyl)(methyl)carbamate

Refernces

• 1、 Iashin, Vladimir,Berta, Dénes,Chernichenko, Konstantin,Nieger, Martin,Moslova, Karina,Pápai, Imre,Repo, Timo. "Metal-Free C?H Borylation of N-Heteroarenes by Boron Trifluoride". supporting information. p. 13873 - 13879. Retrieved 2020/10/02.