2-Azetidinone,4-(acetyloxy)-3-(1-methylethyl)-,(3R-trans)-(9CI)

Base Information

Chemical Name:2-Azetidinone,4-(acetyloxy)-3-(1-methylethyl)-,(3R-trans)-(9CI)
CAS No.:127127-62-2
Molecular Formula:C₈H₁₃NO₃
Molecular Weight:171.196
Hs Code.:
Mol file:127127-62-2.mol

Synonyms:2-Azetidinone,4-(acetyloxy)-3-(1-methylethyl)-,(3R-trans)-(9CI)

Suppliers and Price of 2-Azetidinone,4-(acetyloxy)-3-(1-methylethyl)-,(3R-trans)-(9CI)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of 2-Azetidinone,4-(acetyloxy)-3-(1-methylethyl)-,(3R-trans)-(9CI)

Chemical Property:

PSA：55.40000
LogP:0.60640

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 2-Azetidinone,4-(acetyloxy)-3-(1-methylethyl)-,(3R-trans)-(9CI)

There total 4 articles about 2-Azetidinone,4-(acetyloxy)-3-(1-methylethyl)-,(3R-trans)-(9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 135560-65-5
(3R,4S)-3-isopropyl-4-<(S)-1-<(tert-butyldimethylsilyl)oxy>ethyl>-2-azetidinone

: 127127-62-2,127127-61-1
(3R,4R)-3-isopropyl-4-acetoxy-2-azetidinone

Guidance literature:: Multi-step reaction with 2 steps

1: 98 percent / 40percent aqueous HF / acetonitrile / 1.5 h

2: CaCO₃, lead tetraacetate / benzene / 4 h / Heating

With lead(IV) acetate; hydrogen fluoride; calcium carbonate; In acetonitrile; benzene;
DOI:10.1021/jo00021a007

Reference yield:

: 135560-66-6
(3R,4S)-3-isopropyl-4-<(S)-1-<(tert-butyldimethylsilyl)oxy>phenylmethyl>-2-azetidinone

: 127127-62-2,127127-61-1
(3R,4R)-3-isopropyl-4-acetoxy-2-azetidinone

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / tetrabutylammonium fluoride / tetrahydrofuran / 90 h

2: lead tetraacetate / benzene / 1 h / Heating

With lead(IV) acetate; tetrabutyl ammonium fluoride; In tetrahydrofuran; benzene;
DOI:10.1021/jo00021a007

Reference yield:

: 135560-67-7
(3R,4S)-3-isopropyl-4-<(S)-1-hydroxyethyl>-2-azetidinone

: 127127-64-4
(3R,4S)-3-isopropyl-4-acetoxy-2-azetidinone

: 127127-62-2,127127-61-1
(3R,4R)-3-isopropyl-4-acetoxy-2-azetidinone

Guidance literature:: With lead(IV) acetate; calcium carbonate; In benzene; for 4h; Yield given. Yields of byproduct given. Title compound not separated from byproducts; Heating;
DOI:10.1021/jo00021a007