(4-amino-3-chlorophenyl)(4-methylpiperazin-1-yl)methanone

Base Information

Chemical Name:(4-amino-3-chlorophenyl)(4-methylpiperazin-1-yl)methanone
CAS No.:1378993-22-6
Molecular Formula:C₁₂H₁₆ClN₃O
Molecular Weight:253.732
Hs Code.:
Mol file:1378993-22-6.mol

Synonyms:(4-amino-3-chlorophenyl)(4-methylpiperazin-1-yl)methanone

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Chemical Property of (4-amino-3-chlorophenyl)(4-methylpiperazin-1-yl)methanone

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Technology Process of (4-amino-3-chlorophenyl)(4-methylpiperazin-1-yl)methanone

There total 4 articles about (4-amino-3-chlorophenyl)(4-methylpiperazin-1-yl)methanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: (3-chloro-4-nitrophenyl)(4-methylpiperazin-1-yl)methanone

: 1378993-22-6
(4-amino-3-chlorophenyl)(4-methylpiperazin-1-yl)methanone

Guidance literature:: With iron; ammonium chloride; In ethanol; water; at 80 ℃; for 1h;
DOI:10.1016/j.bmc.2016.07.006

Reference yield:

: 39608-47-4
3-chloro-4-nitrobenzoic acid

: 1378993-22-6
(4-amino-3-chlorophenyl)(4-methylpiperazin-1-yl)methanone

Guidance literature:: Multi-step reaction with 2 steps

1: 4-(4,6-dimethoxy-1,3,5-triazin-2-yl)-4-methylmorpholinium chloride / acetonitrile / 20 °C

2: iron; ammonium chloride / water; ethanol / 1 h / 80 °C

With iron; ammonium chloride; 4-(4,6-dimethoxy-1,3,5-triazin-2-yl)-4-methylmorpholinium chloride; In ethanol; water; acetonitrile;
DOI:10.1016/j.bmc.2016.07.006

Reference yield:

: 109-01-3
1-methyl-piperazine

: 1378993-22-6
(4-amino-3-chlorophenyl)(4-methylpiperazin-1-yl)methanone

Guidance literature:: Multi-step reaction with 2 steps

1: 4-(4,6-dimethoxy-1,3,5-triazin-2-yl)-4-methylmorpholinium chloride / acetonitrile / 20 °C

2: iron; ammonium chloride / water; ethanol / 1 h / 80 °C

With iron; ammonium chloride; 4-(4,6-dimethoxy-1,3,5-triazin-2-yl)-4-methylmorpholinium chloride; In ethanol; water; acetonitrile;
DOI:10.1016/j.bmc.2016.07.006