1-(7-Chloroisoquinolin-2(1H)-yl)ethan-1-one

Base Information

Chemical Name:1-(7-Chloroisoquinolin-2(1H)-yl)ethan-1-one
CAS No.:73261-82-2
Molecular Formula:C₁₁H₁₀ClNO
Molecular Weight:207.659
Hs Code.:
Mol file:73261-82-2.mol

Synonyms:Ethanone, 1-(7-chloro-2(1H)-isoquinolinyl)-;1-(7-Chloroisoquinolin-2(1H)-yl)ethan-1-one

Suppliers and Price of 1-(7-Chloroisoquinolin-2(1H)-yl)ethan-1-one

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Chemenu
1-(7-chloroisoquinolin-2(1H)-yl)ethan-1-one 95%
1g
$ 574.00

Alichem
1-(7-Chloroisoquinolin-2(1H)-yl)ethan-1-one
1g
$ 539.55

Total 5 raw suppliers

Chemical Property of 1-(7-Chloroisoquinolin-2(1H)-yl)ethan-1-one

Chemical Property:

PSA：20.31000
LogP:2.61070
Storage Temp.:2-8°C

Purity/Quality:

95+% ^*data from raw suppliers

1-(7-chloroisoquinolin-2(1H)-yl)ethan-1-one 95% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 1-(7-Chloroisoquinolin-2(1H)-yl)ethan-1-one

There total 3 articles about 1-(7-Chloroisoquinolin-2(1H)-yl)ethan-1-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 73261-76-4
N-(3-chlorobenzyl)-N-(2,2-dimethoxyethyl)acetamide

: 73261-82-2
2-acetyl-7-chloro-1,2-dihydroisoquinoline

Guidance literature:: With aluminium trichloride; In dichloromethane; for 0.166667h; Ambient temperature;
DOI:10.1021/jo01298a038

Reference yield:

: 62882-13-7
N-<(3-chlorophenyl)methylene>-2,2-dimethoxyethanamine

: 73261-82-2
2-acetyl-7-chloro-1,2-dihydroisoquinoline

Guidance literature:: Multi-step reaction with 2 steps

1: 87 percent / H₂ / PtO₂ / ethyl acetate / 1 h / 1034.3 Torr

2: 55 percent / AlCl₃ / CH₂Cl₂ / 0.17 h / Ambient temperature

With aluminium trichloride; hydrogen; platinum(IV) oxide; In dichloromethane; ethyl acetate;
DOI:10.1021/jo01298a038

Reference yield:

: 587-04-2
m-Chlorobenzaldehyde

: 73261-82-2
2-acetyl-7-chloro-1,2-dihydroisoquinoline

Guidance literature:: Multi-step reaction with 3 steps

1: 100 percent / toluene / 1.5 h / Heating

2: 87 percent / H₂ / PtO₂ / ethyl acetate / 1 h / 1034.3 Torr

3: 55 percent / AlCl₃ / CH₂Cl₂ / 0.17 h / Ambient temperature

With aluminium trichloride; hydrogen; platinum(IV) oxide; In dichloromethane; ethyl acetate; toluene;
DOI:10.1021/jo01298a038