1-Methyl-2-phenylhydrazine hydrochloride

Base Information

Chemical Name:1-Methyl-2-phenylhydrazine hydrochloride
CAS No.:92304-54-6
Molecular Formula:C7H11ClN2
Molecular Weight:158.631
Hs Code.:2928000090
DSSTox Substance ID:DTXSID50436613
Mol file:92304-54-6.mol

Synonyms:1-Methyl-2-phenylhydrazine hydrochloride;92304-54-6;1-methyl-2-phenylhydrazine;hydrochloride;1-Methyl-2-phenylhydrazinehydrochloride;SCHEMBL1117892;DTXSID50436613;AMY31165;MFCD09996928;AKOS006303297;1-METHYL-2-PHENYLHYDRAZINE HCL;CS-W007006;DS-5558;SB75862;1-Methyl-2-phenyl-Hydrazine hydrochloride;Hydrazine,1-methyl-2-phenyl-,hydrochloride;C77159;A846563;Hydrazine, 1-methyl-2-phenyl-, hydrochloride (1:1);N-Methylphenylhydrazine hydrochloride

Suppliers and Price of 1-Methyl-2-phenylhydrazine hydrochloride

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Crysdot
1-Methyl-2-phenylhydrazinehydrochloride 98%
1g
$ 260.00

Chemenu
1-methyl-2-phenylhydrazinehydrochloride 95+%
1g
$ 246.00

Ark Pharm
1-Methyl-2-phenylhydrazinehydrochloride 98%
1g
$ 255.00

American Custom Chemicals Corporation
1-METHYL-2-PHENYLHYDRAZINE HYDROCHLORIDE 95.00%
5MG
$ 499.98

Alichem
1-Methyl-2-phenylhydrazinehydrochloride
1g
$ 265.63

AK Scientific
1-Methyl-2-phenylhydrazinehydrochloride
1g
$ 405.00

AK Scientific
1-Methyl-2-phenylhydrazinehydrochloride
250mg
$ 192.00

AK Scientific
1-Methyl-2-phenylhydrazinehydrochloride
100mg
$ 139.00

Total 16 raw suppliers

Chemical Property of 1-Methyl-2-phenylhydrazine hydrochloride

Chemical Property:

Melting Point:160-161℃
PSA：24.06000
LogP:2.49880
Storage Temp.:under inert gas (nitrogen or Argon) at 2-8°C
Hydrogen Bond Donor Count:3
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:2
Exact Mass:158.0610761
Heavy Atom Count:10
Complexity:67.3

Purity/Quality:

97% ^*data from raw suppliers

1-Methyl-2-phenylhydrazinehydrochloride 98% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CNNC1=CC=CC=C1.Cl

Technology Process of 1-Methyl-2-phenylhydrazine hydrochloride

There total 2 articles about 1-Methyl-2-phenylhydrazine hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: tert-butyl 1-methyl-2-phenylhydrazine-1-carboxylate

: 92304-54-6
2-methyl-1-phenylhydrazine hydrochloride

Guidance literature:: With chloro-trimethyl-silane; In methanol; at 4 - 20 ℃; for 3h; Inert atmosphere;
DOI:10.1021/acs.joc.1c00203

Reference yield:

: 108-86-1,52753-63-6
bromobenzene

: 92304-54-6
2-methyl-1-phenylhydrazine hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: copper(l) iodide; N-(2,6-dimethylphenyl)-6-hydroxypicolinamide; potassium carbonate / dimethyl sulfoxide / 8 h / 75 °C / Inert atmosphere

2: chloro-trimethyl-silane / methanol / 3 h / 4 - 20 °C / Inert atmosphere

With copper(l) iodide; chloro-trimethyl-silane; N-(2,6-dimethylphenyl)-6-hydroxypicolinamide; potassium carbonate; In methanol; dimethyl sulfoxide;
DOI:10.1021/acs.joc.1c00203