1-broMo-3-(4-broMophenyl)propane

Base Information

• Chemical Name: 1-broMo-3-(4-broMophenyl)propane
• CAS No.: 90562-10-0
• Molecular Formula: C9H10Br2
• Molecular Weight: 277.986
• Hs Code.: 2903998090
• Mol file: 90562-10-0.mol

Synonyms:1-broMo-3-(4-broMophenyl)propane;1-broMo-4-(3-broMopropyl)benzene

Chemical Property of 1-broMo-3-(4-broMophenyl)propane

Chemical Property:

• PSA: 0.00000
• LogP: 3.77660
• Storage Temp.: Sealed in dry,Room Temperature

Purity/Quality:

98.5% ^*data from raw suppliers

1-Bromo-4-(3-bromopropyl)benzene 95% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1-broMo-3-(4-broMophenyl)propane

There total 9 articles about 1-broMo-3-(4-broMophenyl)propane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

3-(4-bromophenyl)propanol (25574-11-2) → trans-1-(3-bromopropyl)-4-bromobenzene (90562-10-0)

Guidance literature:

With N-Bromosuccinimide; triphenylphosphine; In dichloromethane; at 0 ℃; for 1h; Inert atmosphere;

DOI:10.1002/chem.201805938

Reference yield: 70.0%

1-bromo-4-cyclopropylbenzene (1124-14-7) → trans-1-(3-bromopropyl)-4-bromobenzene (90562-10-0)

Guidance literature:

With boron tribromide; tert-butyl alcohol; In dichloromethane; at 23 ℃; for 25h; regioselective reaction;

DOI:10.1039/d0sc02567d

Reference yield: 41.0%

→ trans-1-(3-bromopropyl)-4-bromobenzene (90562-10-0)

Guidance literature:

With phosphorus tribromide; In 1,4-dioxane; at 10 - 20 ℃; Inert atmosphere;

upstream raw materials:

3-(4-bromophenyl)propanol

3-(4-bromo-phenyl)-propionic acid ethyl ester

3-(4-bromophenyl)acrylic acid

4-bromo-benzaldehyde

Downstream raw materials:

O-(3-(4-deuteriophenyl)propyl) acetohydroxamate

N-chloro-O-(3-(4-deuteriophenyl)propyl) acetohydroxamate

O-(3-(4-deuteriophenyl)propyl) benzohydroxamate

N-chloro-O-(3-(4-deuteriophenyl)propyl) benzohydroxamate