Technology Process of 3,6-bis(5-broMo-4-(2-ethylhexyl)thiophen-2-yl)-1,2,4,5-tetrazine
There total 6 articles about 3,6-bis(5-broMo-4-(2-ethylhexyl)thiophen-2-yl)-1,2,4,5-tetrazine which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
N-Bromosuccinimide; acetic acid;
In
chloroform;
at 20 - 80 ℃;
DOI:10.1039/c0cc02766a
- Guidance literature:
-
Multi-step reaction with 2 steps
1: isopentyl nitrite / chloroform / 20 °C
2: N-Bromosuccinimide; acetic acid / chloroform / 80 °C
With
N-Bromosuccinimide; acetic acid; isopentyl nitrite;
In
chloroform;
DOI:10.1021/cm200330c
- Guidance literature:
-
Multi-step reaction with 5 steps
1: pyridine; hydroxylamine hydrochloride / ethanol / 80 °C
2: potassium acetate / acetic anhydride / 150 °C
3: sulfur; hydrazine hydrate / ethanol / 20 °C / Reflux
4: isopentyl nitrite / chloroform / 20 °C
5: N-Bromosuccinimide; acetic acid / chloroform / 80 °C
With
pyridine; N-Bromosuccinimide; hydroxylamine hydrochloride; potassium acetate; sulfur; hydrazine hydrate; acetic acid; isopentyl nitrite;
In
ethanol; chloroform; acetic anhydride;
3: Pinner amidine synthesis;
DOI:10.1021/cm200330c