3-(pyridin-3-yl)cyclohexanamine

Base Information

Chemical Name:3-(pyridin-3-yl)cyclohexanamine
CAS No.:933700-52-8
Molecular Formula:C₁₁H₁₆N₂
Molecular Weight:176.261
Hs Code.:

Synonyms:3-(pyridin-3-yl)cyclohexanamine

Suppliers and Price of 3-(pyridin-3-yl)cyclohexanamine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-(pyridin-3-yl)cyclohexanamine

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 3-(pyridin-3-yl)cyclohexanamine

There total 5 articles about 3-(pyridin-3-yl)cyclohexanamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1261225-81-3
C₁₁H₁₄N₂O

: 933700-52-8
trans-3-(3-pyridyl)cyclohexylamine

Guidance literature:: C₁₁H₁₄N₂O; With lithium aluminium tetrahydride; In tetrahydrofuran; at 0 ℃;

With sodium hydroxide; In tetrahydrofuran; water;

Reference yield:

: 63843-14-1
3-(3-pyridinyl)-2-cyclohexen-1-one

: 933700-52-8
trans-3-(3-pyridyl)cyclohexylamine

Guidance literature:: Multi-step reaction with 3 steps

1: hydrogen / Rh/Al₂O₃ / ethanol / 20 °C / 760.05 Torr

2: potassium carbonate; hydroxylamine hydrochloride / water; methanol

3: lithium aluminium tetrahydride / tetrahydrofuran / 0 °C

With lithium aluminium tetrahydride; hydroxylamine hydrochloride; hydrogen; potassium carbonate; Rh/Al₂O₃; In tetrahydrofuran; methanol; ethanol; water;

Reference yield:

: 504-02-9
1,3-cylohexanedione

: 933700-52-8
trans-3-(3-pyridyl)cyclohexylamine

Guidance literature:: Multi-step reaction with 5 steps

1: N,N-dimethyl-formamide; oxalyl dichloride / dichloromethane / 0 °C

2: sodium carbonate / dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂ / 1,4-dioxane; water / 7 h / 95 °C / Inert atmosphere

3: hydrogen / Rh/Al₂O₃ / ethanol / 20 °C / 760.05 Torr

4: potassium carbonate; hydroxylamine hydrochloride / water; methanol

5: lithium aluminium tetrahydride / tetrahydrofuran / 0 °C

With lithium aluminium tetrahydride; oxalyl dichloride; hydroxylamine hydrochloride; hydrogen; sodium carbonate; potassium carbonate; N,N-dimethyl-formamide; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; Rh/Al₂O₃; In tetrahydrofuran; 1,4-dioxane; methanol; ethanol; dichloromethane; water;