2H-Pyran-3-amine,3,6-dihydro-6-(1-methylethoxy)-,(3R,6S)-(9CI)

Base Information

Chemical Name:2H-Pyran-3-amine,3,6-dihydro-6-(1-methylethoxy)-,(3R,6S)-(9CI)
CAS No.:405145-96-2
Molecular Formula:C₈H₁₅NO₂
Molecular Weight:157.213
Hs Code.:
Mol file:405145-96-2.mol

Synonyms:2H-Pyran-3-amine,3,6-dihydro-6-(1-methylethoxy)-,(3R,6S)-(9CI)

Suppliers and Price of 2H-Pyran-3-amine,3,6-dihydro-6-(1-methylethoxy)-,(3R,6S)-(9CI)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2H-Pyran-3-amine,3,6-dihydro-6-(1-methylethoxy)-,(3R,6S)-(9CI)

Chemical Property:

PSA：44.48000
LogP:1.35150

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 2H-Pyran-3-amine,3,6-dihydro-6-(1-methylethoxy)-,(3R,6S)-(9CI)

There total 4 articles about 2H-Pyran-3-amine,3,6-dihydro-6-(1-methylethoxy)-,(3R,6S)-(9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 405145-93-9
isopropyl β-L-4-azido-2,3,4-trideoxypent-2-enoglyceropyranoside

: 405145-96-2
isopropyl β-L-4-amino-2,3,4-trideoxypent-2-enoglyceropyranoside

Guidance literature:: With lithium aluminium tetrahydride; In tetrahydrofuran; at 0 ℃; for 2h;
DOI:10.1016/S0957-4166(01)00450-5

Reference yield:

: 357282-68-9
isopropyl β-D-2,3-dideoxypent-2-enoglyceropyranoside

: 405145-96-2
isopropyl β-L-4-amino-2,3,4-trideoxypent-2-enoglyceropyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 95 percent / triethylamine; DMAP / ethyl acetate / 3 h / 0 °C

2: 81 percent / Amberlite IRA-900 in azide form / benzene / 2 h / Heating

3: 87 percent / LiAlH₄ / tetrahydrofuran / 2 h / 0 °C

With dmap; lithium aluminium tetrahydride; Amberlite IRA-900 in azide form; triethylamine; In tetrahydrofuran; ethyl acetate; benzene;
DOI:10.1016/S0957-4166(01)00450-5

Reference yield:

: 357282-70-3
isopropyl β-D-4-O-acetyl-2,3-dideoxypent-2-enoglyceropyranoside

: 405145-96-2
isopropyl β-L-4-amino-2,3,4-trideoxypent-2-enoglyceropyranoside

Guidance literature:: Multi-step reaction with 4 steps

1: 100 percent / resin IRA 900 in the methoxide form / methanol / 1 h / 20 °C

2: 95 percent / triethylamine; DMAP / ethyl acetate / 3 h / 0 °C

3: 81 percent / Amberlite IRA-900 in azide form / benzene / 2 h / Heating

4: 87 percent / LiAlH₄ / tetrahydrofuran / 2 h / 0 °C

With dmap; lithium aluminium tetrahydride; Amberlite IRA-900 in azide form; resin IRA 900 in the methoxide form; triethylamine; In tetrahydrofuran; methanol; ethyl acetate; benzene;
DOI:10.1016/S0957-4166(01)00450-5