2-(N-isopropylphenylsulfonaMido)acetic acid

Base Information

• Chemical Name: 2-(N-isopropylphenylsulfonaMido)acetic acid
• CAS No.: 1033194-55-6
• Molecular Formula: C11H15NO4S
• Molecular Weight: 257.3061
• Mol file: 1033194-55-6.mol

Synonyms:2-(N-isopropylphenylsulfonaMido)acetic acid;(Benzenesulfonyl-isopropyl-amino)-acetic acid

Chemical Property of 2-(N-isopropylphenylsulfonaMido)acetic acid

Chemical Property:

• PSA: 83.06000
• LogP: 2.25110
• Storage Temp.: 2-8°C

Purity/Quality:

97% ^*data from raw suppliers

2-(N-Isopropylphenylsulfonamido)aceticAcid ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-(N-isopropylphenylsulfonaMido)acetic acid

There total 2 articles about 2-(N-isopropylphenylsulfonaMido)acetic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(benzenesulfonyl(isopropyl)amino)acetic acid tert-butyl ester (1590397-98-0) → (benzenesulfonyl(isopropyl)amino)acetic acid (1033194-55-6)

Guidance literature:

With hydrogenchloride; In 1,4-dioxane; for 14h;

Reference yield:

isopropylamino-acetic acid tert-butyl ester (127983-07-7) → (benzenesulfonyl(isopropyl)amino)acetic acid (1033194-55-6)

Guidance literature:

Multi-step reaction with 2 steps

1: triethylamine / dichloromethane / 4 h / 20 °C

2: hydrogenchloride / 1,4-dioxane / 14 h

With hydrogenchloride; triethylamine; In 1,4-dioxane; dichloromethane;

Reference yield:

[3-[4-(trifluoromethyl)phenyl] phenyl]methanamine (472964-40-2) + (benzenesulfonyl(isopropyl)amino)acetic acid (1033194-55-6) → 2-(benzenesulfonylisopropylamino)-N-(4'-trifluoromethylbiphenyl-3-ylmethyl)acetamide (1590397-35-5)

Guidance literature:

With N-ethyl-N,N-diisopropylamine; HATU; In dichloromethane; at 20 ℃; for 16h;

upstream raw materials:

isopropylamino-acetic acid tert-butyl ester

(benzenesulfonyl(isopropyl)amino)acetic acid tert-butyl ester

Downstream raw materials:

2-(benzenesulfonylisopropylamino)-N-(4'-trifluoromethylbiphenyl-3-ylmethyl)acetamide

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