2,3',4',5'-Tetrafluoro-4-(4'-propyl-[1,1'-bi(cyclohexan)]-4-yl)-1,1'-biphenyl

Base Information

Chemical Name:2,3',4',5'-Tetrafluoro-4-(4'-propyl-[1,1'-bi(cyclohexan)]-4-yl)-1,1'-biphenyl
CAS No.:188289-44-3
Molecular Formula:
Molecular Weight:0
Hs Code.:
European Community (EC) Number:606-136-2
DSSTox Substance ID:DTXSID201019868
Nikkaji Number:J2.566.029C

Synonyms:2,3',4',5'-Tetrafluoro-4-(4'-propyl-[1,1'-bi(cyclohexan)]-4-yl)-1,1'-biphenyl;188289-44-3;2757730-17-7;1,1'-Biphenyl, 2,3',4',5'-tetrafluoro-4-[(trans,trans)-4'-propyl[1,1'-bicyclohexyl]-4-yl]-;SCHEMBL1754930;SCHEMBL18472161;RHJZNALCKPDGPQ-UBBSCCEASA-N;RHJZNALCKPDGPQ-UHFFFAOYSA-N;DTXSID201019868;BS-48797;F71396;1,2,3-trifluoro-5-[2-fluoro-4-[4-(4-propylcyclohexyl)cyclohexyl]phenyl]benzene

Suppliers and Price of 2,3',4',5'-Tetrafluoro-4-(4'-propyl-[1,1'-bi(cyclohexan)]-4-yl)-1,1'-biphenyl

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 15 raw suppliers

Chemical Property of 2,3',4',5'-Tetrafluoro-4-(4'-propyl-[1,1'-bi(cyclohexan)]-4-yl)-1,1'-biphenyl

Chemical Property:

Vapor Pressure:8.42E-09mmHg at 25°C
Boiling Point:476.9°C at 760 mmHg
Flash Point:220.2°C
Density:1.117g/cm³
XLogP3:10.3
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:5
Exact Mass:432.24401367
Heavy Atom Count:31
Complexity:525

Purity/Quality:: 99.9% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CCCC1CCC(CC1)C2CCC(CC2)C3=CC(=C(C=C3)C4=CC(=C(C(=C4)F)F)F)F

Technology Process of 2,3',4',5'-Tetrafluoro-4-(4'-propyl-[1,1'-bi(cyclohexan)]-4-yl)-1,1'-biphenyl

There total 4 articles about 2,3',4',5'-Tetrafluoro-4-(4'-propyl-[1,1'-bi(cyclohexan)]-4-yl)-1,1'-biphenyl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₅H₁₂F₄Mg

: trans-4-(trans-4'-n-propylcyclohexyl)cyclohexan-4-one

: 188289-44-3,2757730-17-7
4-(trans,trans-4-propylbicyclohexyl)-2,3’4’,5’-tetrafluorobiphenyl

Guidance literature:: C₁₅H₁₂F₄Mg; trans-4-(trans-4'-n-propylcyclohexyl)cyclohexan-4-one; In tetrahydrofuran; at 50 ℃; for 2h;

With 5%-palladium/activated carbon; hydrogen; In ethanol;

Reference yield:

: 143418-49-9
3,4,5-trifluorophenylboronic acid

: 188289-44-3,2757730-17-7
4-(trans,trans-4-propylbicyclohexyl)-2,3’4’,5’-tetrafluorobiphenyl

Guidance literature:: Multi-step reaction with 4 steps

1.1: potassium carbonate; bis(di-tert-?butyl(4-?dimethylaminophenyl)?phosphine)?dichloropalladium(II) / N,N-dimethyl-formamide; water / 6 h / Reflux; Inert atmosphere

2.1: sodium nitrite / water / 0.25 h / -10 - 0 °C

2.2: 10 h / 0 °C

3.1: tetrahydrofuran / 3 h / 0 - 50 °C

4.1: tetrahydrofuran / 2 h / 50 °C

With bis(di-tert-?butyl(4-?dimethylaminophenyl)?phosphine)?dichloropalladium(II); potassium carbonate; sodium nitrite; In tetrahydrofuran; water; N,N-dimethyl-formamide;

Reference yield:

: 656-65-5
3-fluoro-4-bromophenylamine

: 188289-44-3,2757730-17-7
4-(trans,trans-4-propylbicyclohexyl)-2,3’4’,5’-tetrafluorobiphenyl

Guidance literature:: Multi-step reaction with 4 steps

1.1: potassium carbonate; bis(di-tert-?butyl(4-?dimethylaminophenyl)?phosphine)?dichloropalladium(II) / N,N-dimethyl-formamide; water / 6 h / Reflux; Inert atmosphere

2.1: sodium nitrite / water / 0.25 h / -10 - 0 °C

2.2: 10 h / 0 °C

3.1: tetrahydrofuran / 3 h / 0 - 50 °C

4.1: tetrahydrofuran / 2 h / 50 °C

With bis(di-tert-?butyl(4-?dimethylaminophenyl)?phosphine)?dichloropalladium(II); potassium carbonate; sodium nitrite; In tetrahydrofuran; water; N,N-dimethyl-formamide;