Methyl 3-bromo-2-(bromomethyl)-4,5-dimethoxybenzoate

Base Information

• Chemical Name: Methyl 3-bromo-2-(bromomethyl)-4,5-dimethoxybenzoate
• CAS No.: 1042722-41-7
• Molecular Formula: C11H12Br2O4
• Molecular Weight: 368.022
• Hs Code.: 2918990090
• Mol file: 1042722-41-7.mol

Synonyms:Methyl 3-bromo-2-(bromomethyl)-4,5-dimethoxybenzoate

Chemical Property of Methyl 3-bromo-2-(bromomethyl)-4,5-dimethoxybenzoate

Chemical Property:

• Melting Point: 126 °C
• Boiling Point: 414.5±45.0 °C(Predicted)
• PSA: 44.76000
• Density: 1.665±0.06 g/cm3(Predicted)
• LogP: 3.14780

Purity/Quality:

98% ^*data from raw suppliers

Methyl3-bromo-2-(bromomethyl)-4,5-dimethoxybenzoate 95+% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Methyl 3-bromo-2-(bromomethyl)-4,5-dimethoxybenzoate

There total 1 articles about Methyl 3-bromo-2-(bromomethyl)-4,5-dimethoxybenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

methyl 3-bromo-4,5-dimethoxy-2-methylbenzoate (1042722-40-6) → methyl 3-bromo-2-bromomethyl-4,5-dimethoxybenzoate (1042722-41-7)

Guidance literature:

With N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile); In benzene; at 80 ℃; for 1h;

DOI:10.1021/ol801291k

Reference yield: 98.0%

methyl 3-bromo-2-bromomethyl-4,5-dimethoxybenzoate (1042722-41-7) + aminothioanisole → C17H16BrNO3S

Guidance literature:

In tetrahydrofuran; at 20 ℃;

DOI:10.1016/j.bmcl.2009.04.020

Reference yield: 93.0%

methyl 3-bromo-2-bromomethyl-4,5-dimethoxybenzoate (1042722-41-7) + methyl 4-(aminomethyl)benzoate hydrochloride (6232-11-7) → methyl 4-((4-bromo-5,6-dimethoxy-1-oxoisoindolin-2-yl)methyl)-benzoate (1255951-59-7)

Guidance literature:

With triethylamine; In tetrahydrofuran; water; at 20 ℃;

upstream raw materials:

methyl 3-bromo-4,5-dimethoxy-2-methylbenzoate

Downstream raw materials:

4-bromo-2-(4-t-butylphenyl)-5,6-dimethoxyisoindolin-1-one

4-bromo-5,6-dimethoxy-2-(4-methoxyphenyl)isoindolin-1-one

4-bromo-5,6-dimethoxy-2-phenethylisoindolin-1-one

methyl 4-((4-bromo-5,6-dimethoxy-1-oxoisoindolin-2-yl)methyl)-benzoate

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