1H-Pyrrole-1,2-dicarboxylic acid, 2,3-dihydro-, dimethyl ester (9CI)

Base Information

Chemical Name:1H-Pyrrole-1,2-dicarboxylic acid, 2,3-dihydro-, dimethyl ester (9CI)
CAS No.:440367-12-4
Molecular Formula:C₈H₁₁NO₄
Molecular Weight:185.18
Hs Code.:
Mol file:440367-12-4.mol

Synonyms:1H-Pyrrole-1,2-dicarboxylic acid, 2,3-dihydro-, dimethyl ester (9CI)

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Chemical Property of 1H-Pyrrole-1,2-dicarboxylic acid, 2,3-dihydro-, dimethyl ester (9CI)

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Technology Process of 1H-Pyrrole-1,2-dicarboxylic acid, 2,3-dihydro-, dimethyl ester (9CI)

There total 7 articles about 1H-Pyrrole-1,2-dicarboxylic acid, 2,3-dihydro-, dimethyl ester (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 185385-13-1
1-carbomethoxy-5-methoxy-L-proline methyl ester

: 83487-05-2,440367-12-4
N-carbomethoxy-4,5-dehydroproline methyl ester

Guidance literature:: With ammonium chloride; for 1h; under 20 - 100 Torr; Heating;
DOI:10.1021/ja00388a037

Reference yield: 70.0%

: 185385-13-1
1-carbomethoxy-5-methoxy-L-proline methyl ester

: 83487-05-2,440367-12-4
(5S)-N-(methoxycarbonyl)-5-(methoxycarbonyl)-2-pyrroline

Guidance literature:: With ammonium chloride; Heating;
DOI:10.1039/c39830001169

Reference yield: 46.0%

: 93271-96-6
(2S,5RS)-1,2-dimethyl-5-hydroxypyrrolidine-1,2-dicarboxylate

: 83487-05-2,440367-12-4
(5S)-N-(methoxycarbonyl)-5-(methoxycarbonyl)-2-pyrroline

Guidance literature:: (2S,5RS)-1,2-dimethyl-5-hydroxypyrrolidine-1,2-dicarboxylate; With 2,6-dimethylpyridine; trifluoroacetic anhydride; In toluene; at 0 ℃; for 7h;

for 0.333333h; Heating;
DOI:10.1021/jo9903297