9-benzyl-11-iodo-1,4-dioxa-9-azadispiro[4.2.48.25]tetradecane

Base Information

Chemical Name:9-benzyl-11-iodo-1,4-dioxa-9-azadispiro[4.2.48.25]tetradecane
CAS No.:635728-14-2
Molecular Formula:C₁₈H₂₄INO₂
Molecular Weight:413.299
Hs Code.:

Synonyms:9-benzyl-11-iodo-1,4-dioxa-9-azadispiro[4.2.48.25]tetradecane;9-Benzyl-11-iodo-1,4-dioxa-9-azadispiro[4.2.4.2]tetradecane

Suppliers and Price of 9-benzyl-11-iodo-1,4-dioxa-9-azadispiro[4.2.48.25]tetradecane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 5 raw suppliers

Chemical Property of 9-benzyl-11-iodo-1,4-dioxa-9-azadispiro[4.2.48.25]tetradecane

Chemical Property:

Purity/Quality:: 97% ^*data from raw suppliers

Safty Information:

Pictogram(s):
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Technology Process of 9-benzyl-11-iodo-1,4-dioxa-9-azadispiro[4.2.48.25]tetradecane

There total 2 articles about 9-benzyl-11-iodo-1,4-dioxa-9-azadispiro[4.2.48.25]tetradecane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 635728-13-1
4-allyl-4-benzylaminocyclohexanone ethylene acetal

: 635728-14-2
1-benzyl-3-iodo-1-azaspiro[4.5]decan-8-one ethylene acetal

Guidance literature:: With iodine; sodium hydrogencarbonate; In dichloromethane; at 20 ℃;
DOI:10.1002/ejoc.200700056

Reference yield:

: 230287-23-7
N-(1,4-dioxaspiro[4.5]decyl-7-idene)benzylamine

: 635728-14-2
1-benzyl-3-iodo-1-azaspiro[4.5]decan-8-one ethylene acetal

Guidance literature:: Multi-step reaction with 2 steps

1: 70 percent / I₂; NaHCO₃ / H₂O; tetrahydrofuran / 20 °C

With iodine; sodium hydrogencarbonate; In tetrahydrofuran; water;
DOI:10.1016/j.tetlet.2003.09.111