Technology Process of COPPER(II) TETRAKIS(4-CUMYLPHENOXY)-
There total 1 articles about COPPER(II) TETRAKIS(4-CUMYLPHENOXY)- which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
catalyst: 1,8-diazabicyclo [5.4.0] undec-7-ene;
In
neat (no solvent);
Irradiation (UV/VIS); 4-cumylphenoxy-4-phthalonitrile (2.96 mmol) and CuCl2 (1.49 mmol) in thepresence of DBU were irradiated in a quartz vessel by a microwave oven at 440 W for 10 min; the complex was washed with a methanol/water soln.; column chromy. (silica gel, tetrahydrofuran/ethyl acetate/methanol = 4/1/1, wt./wt./wt.); the complex was dried; elem. anal.;
DOI:10.1016/j.jorganchem.2004.01.017