3'-Deoxy-N,N-dimethyl-3'-(benzylamino)adenosine

Base Information

Chemical Name:3'-Deoxy-N,N-dimethyl-3'-(benzylamino)adenosine
CAS No.:36913-17-4
Molecular Formula:C19H24N6O3
Molecular Weight:384.438
Hs Code.:
Mol file:36913-17-4.mol

Synonyms:3'-Deoxy-N,N-dimethyl-3'-(benzylamino)adenosine

Suppliers and Price of 3'-Deoxy-N,N-dimethyl-3'-(benzylamino)adenosine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of 3'-Deoxy-N,N-dimethyl-3'-(benzylamino)adenosine

Chemical Property:

PSA：108.56000
LogP:0.69220

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 3'-Deoxy-N,N-dimethyl-3'-(benzylamino)adenosine

There total 5 articles about 3'-Deoxy-N,N-dimethyl-3'-(benzylamino)adenosine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.3%

: 934011-54-8
9-[3-(benzylamino)-3-N,2-O-carbonyl-3-deoxy-β-D-ribofuranosyl]-N⁶,N⁶-dimethyladenine

: 36913-17-4
4-benzylamino-2-(6-dimethylamino-purin-9-yl)-5-hydroxymethyl-tetrahydro-furan-3-ol

Guidance literature:: With sodium hydroxide; In various solvent(s); at 20 ℃; for 96h;
DOI:10.1080/15257770600725929

Reference yield:

: 934011-52-6
9-[2-O-(N-benzylcarbamoyl)-3,5-O-sulfinyl-β-D-xylofuranosyl]-N⁶,N⁶-dimethyladenine

: 36913-17-4
4-benzylamino-2-(6-dimethylamino-purin-9-yl)-5-hydroxymethyl-tetrahydro-furan-3-ol

Guidance literature:: Multi-step reaction with 2 steps

1: NaH; dipotassium hydrogenphosphate / dimethylformamide / 20 h / -30 °C

2: 70.3 percent / aq. NaOH / various solvent(s) / 96 h / 20 °C

With sodium hydroxide; dipotassium hydrogenphosphate; sodium hydride; In N,N-dimethyl-formamide;
DOI:10.1080/15257770600725929

Reference yield:

: 669055-52-1
9-(β-D-xylofuranosyl)-N⁶,N⁶-dimethyladenine

: 36913-17-4
4-benzylamino-2-(6-dimethylamino-purin-9-yl)-5-hydroxymethyl-tetrahydro-furan-3-ol

Guidance literature:: Multi-step reaction with 4 steps

1: 75 percent / thionyl chloride; pyridine / acetonitrile / 8 h / 25 °C

2: 98.5 percent / Et₃N / tetrahydrofuran; acetonitrile / 21 h / 25 °C

3: NaH; dipotassium hydrogenphosphate / dimethylformamide / 20 h / -30 °C

4: 70.3 percent / aq. NaOH / various solvent(s) / 96 h / 20 °C

With pyridine; sodium hydroxide; dipotassium hydrogenphosphate; thionyl chloride; sodium hydride; triethylamine; In tetrahydrofuran; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1080/15257770600725929