HEXADECANE,7,9-DIMETHYL-

Base Information

Chemical Name:HEXADECANE,7,9-DIMETHYL-
CAS No.:21164-95-4
Molecular Formula:C₁₈H₃₈
Molecular Weight:254.5
Hs Code.:
Mol file:21164-95-4.mol

Synonyms:HEXADECANE,7,9-DIMETHYL-

Suppliers and Price of HEXADECANE,7,9-DIMETHYL-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemicals and raw materials
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price

Total 3 raw suppliers

Chemical Property of HEXADECANE,7,9-DIMETHYL-

Chemical Property:

Boiling Point:297.9±7.0 °C(Predicted)
PSA：0.00000
Density:0.779±0.06 g/cm3(Predicted)
LogP:0.00000

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

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Technology Process of HEXADECANE,7,9-DIMETHYL-

There total 28 articles about HEXADECANE,7,9-DIMETHYL- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 3067-88-7
3,5-dimethylcaprolactone

: 21164-95-4
7,9-dimethylhexadecane

Guidance literature:: Multi-step reaction with 12 steps

1.1: 93 percent / methanol / 3.5 h

2.1: 79 percent / TsOH / CH₂Cl₂ / 4 h

3.1: 85 percent / LiAlH₄ / diethyl ether / 2 h

4.1: 85 percent / 4-methylmorpholine N-oxide; tetrapropylammonium perruthenate / CH₂Cl₂ / 6 h

5.1: Mg; iodine / diethyl ether / 0.5 h / Heating

5.2: 83 percent / diethyl ether / 0.25 h

6.1: triethylamine / CH₂Cl₂ / 1 h

7.1: 1.0 g / LiAlH₄ / diethyl ether / 2 h / Heating

8.1: 97 percent / p-toluenesulfonic acid / methanol / 2 h

9.1: 4-methylmorpholine N-oxide; tetrapropylammonium perruthenate / CH₂Cl₂ / 6 h

10.1: Mg / diethyl ether / Heating

10.2: 85 percent / diethyl ether

11.1: triethylamine / CH₂Cl₂

12.1: LiAlH₄ / diethyl ether / Heating

With lithium aluminium tetrahydride; tetrapropylammonium perruthennate; iodine; toluene-4-sulfonic acid; magnesium; 4-methylmorpholine N-oxide; triethylamine; In methanol; diethyl ether; dichloromethane;
DOI:10.1021/jo0481093

Reference yield:

: 3067-88-7
3,5-dimethylcaprolactone

: 21164-95-4
7,9-dimethylhexadecane

Guidance literature:: Multi-step reaction with 12 steps

1.1: 93 percent / methanol / 3.5 h

2.1: 79 percent / TsOH / CH₂Cl₂ / 4 h

3.1: 85 percent / LiAlH₄ / diethyl ether / 2 h

4.1: 85 percent / 4-methylmorpholine N-oxide; tetrapropylammonium perruthenate / CH₂Cl₂ / 6 h

5.1: Mg; iodine / diethyl ether / 0.5 h / Heating

5.2: 83 percent / diethyl ether / 0.25 h

6.1: triethylamine / CH₂Cl₂ / 1 h

7.1: 1.0 g / LiAlH₄ / diethyl ether / 2 h / Heating

8.1: 97 percent / p-toluenesulfonic acid / methanol / 2 h

9.1: 4-methylmorpholine N-oxide; tetrapropylammonium perruthenate / CH₂Cl₂ / 6 h

10.1: Mg / diethyl ether / Heating

10.2: 85 percent / diethyl ether

11.1: triethylamine / CH₂Cl₂

12.1: LiAlH₄ / diethyl ether / Heating

With lithium aluminium tetrahydride; tetrapropylammonium perruthennate; iodine; toluene-4-sulfonic acid; magnesium; 4-methylmorpholine N-oxide; triethylamine; In methanol; diethyl ether; dichloromethane;
DOI:10.1021/jo0481093

Reference yield:

: 2320-30-1
3,5-dimethylcyclohexanone

: 21164-95-4
7,9-dimethylhexadecane

Guidance literature:: Multi-step reaction with 13 steps

1.1: 74 percent / m-chloroperbenzoic acid; NaHCO₃ / CH₂Cl₂ / 6 h

2.1: 93 percent / methanol / 3.5 h

3.1: 79 percent / TsOH / CH₂Cl₂ / 4 h

4.1: 85 percent / LiAlH₄ / diethyl ether / 2 h

5.1: 85 percent / 4-methylmorpholine N-oxide; tetrapropylammonium perruthenate / CH₂Cl₂ / 6 h

6.1: Mg; iodine / diethyl ether / 0.5 h / Heating

6.2: 83 percent / diethyl ether / 0.25 h

7.1: triethylamine / CH₂Cl₂ / 1 h

8.1: 1.0 g / LiAlH₄ / diethyl ether / 2 h / Heating

9.1: 97 percent / p-toluenesulfonic acid / methanol / 2 h

10.1: 4-methylmorpholine N-oxide; tetrapropylammonium perruthenate / CH₂Cl₂ / 6 h

11.1: Mg / diethyl ether / Heating

11.2: 85 percent / diethyl ether

12.1: triethylamine / CH₂Cl₂

13.1: LiAlH₄ / diethyl ether / Heating

With lithium aluminium tetrahydride; tetrapropylammonium perruthennate; iodine; sodium hydrogencarbonate; toluene-4-sulfonic acid; magnesium; 4-methylmorpholine N-oxide; triethylamine; 3-chloro-benzenecarboperoxoic acid; In methanol; diethyl ether; dichloromethane; 1.1: Baeyer-Villiger oxidation;
DOI:10.1021/jo0481093