2,7-Dichlorofluorenyl BroMoMethyl Ketone

Base Information

• Chemical Name: 2,7-Dichlorofluorenyl BroMoMethyl Ketone
• CAS No.: 53221-22-0
• Molecular Formula: C15H9BrCl2O
• Molecular Weight: 356.046
• Mol file: 53221-22-0.mol

Synonyms:2,7-Dichlorofluorenyl BroMoMethyl Ketone;2-BroMo-1-(2,7-dichloro-9H-fluoren-4-yl)ethanone;BroMoMethyl 2,7-Dichloro-4-fluorenyl Ketone

Chemical Property of 2,7-Dichlorofluorenyl BroMoMethyl Ketone

Chemical Property:

• PSA: 17.07000
• LogP: 5.14220

Purity/Quality:

98%Min ^*data from raw suppliers

2,7-DichlorofluorenylBromomethylKetone ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Uses: Intermediate in the preparation of Antimalarials.

Technology Process of 2,7-Dichlorofluorenyl BroMoMethyl Ketone

There total 3 articles about 2,7-Dichlorofluorenyl BroMoMethyl Ketone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2,7-Dichlor-fluoren-carbonsaeure-(4) (53221-16-2) → Brommethyl-2,7-dichlor-4-fluorenyl-keton (53221-22-0)

Guidance literature:

Multi-step reaction with 2 steps

1: SOCl₂

2: (i), (ii) HBr, Et₂O

With thionyl chloride;

DOI:10.1021/jm00255a022

Reference yield:

2,7-dichloro-9-oxo-fluorene-4-carboxylic acid (53221-15-1) → Brommethyl-2,7-dichlor-4-fluorenyl-keton (53221-22-0)

Guidance literature:

Multi-step reaction with 3 steps

1: (reduction)

2: SOCl₂

3: (i), (ii) HBr, Et₂O

With thionyl chloride;

DOI:10.1021/jm00255a022

Reference yield:

diazomethane (186581-53-3,908094-01-9,334-88-3) + 2,7-Dichlorfluoren-4-carbonsaeurechlorid (53221-17-3) → Brommethyl-2,7-dichlor-4-fluorenyl-keton (53221-22-0)

Guidance literature:

Multistep reaction; (i), (ii) HBr, Et₂O;

DOI:10.1021/jm00255a022

upstream raw materials:

diazomethane

2,7-Dichlorfluoren-4-carbonsaeurechlorid

2,7-Dichlor-fluoren-carbonsaeure-⁽⁴⁾

2,7-dichloro-9-oxo-fluorene-4-carboxylic acid

Downstream raw materials:

C₂₅H₁₈Cl₂N₄O₂S₂

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