ZIRCONIUM DIPERCHLORATE OXIDE OCTAHYDRATE

Base Information

• Chemical Name: ZIRCONIUM DIPERCHLORATE OXIDE OCTAHYDRATE
• CAS No.: 12591-05-8
• Molecular Formula: 2ClO₄*OZr
• Molecular Weight: 306.125
• Mol file: 12591-05-8.mol

Synonyms:ZIRCONIUM DIPERCHLORATE OXIDE OCTAHYDRATE;ZIRCONIUM(IV)DIPERCHLORATE OXIDE OCTAHYDRATE;ZIRCONIUM OXIDE DIPERCHLORATE;ZIRCONYL PERCHLORATE;ZIRCONYL PERCHLORATE HYDRATE;ZIRCONYL PERCHLORATE, HYDRATED;ZIRCONYL PERCHLORATE OCTAHYDRATE;ZIRCONYL PERCHLORATE, HYDRATED REAGENT

Chemical Property of ZIRCONIUM DIPERCHLORATE OXIDE OCTAHYDRATE

Chemical Property:

Purity/Quality:

98%Min ^*data from raw suppliers

Safty Information:

• Hazard Codes: O,Xi
• Statements: 36/37/38
• Safety Statements: 26-36

MSDS Files:

Useful:

Technology Process of ZIRCONIUM DIPERCHLORATE OXIDE OCTAHYDRATE

There total 1 articles about ZIRCONIUM DIPERCHLORATE OXIDE OCTAHYDRATE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

perchloric acid (7601-90-3) → zirconiumoxide perchlorate (12591-05-8,15607-09-7)

Guidance literature:

With Zirkonoxydhydrogel (germ.); In water; 25% HClO4 is used;; evapn. and cooling;;

Reference yield:

zirconiumoxide perchlorate (12591-05-8,15607-09-7) + Dibenzyl sulfoxide (621-08-9) → ZrO(2+)*2ClO4(1-)*6(C6H5CH2)2SO=ZrO(ClO4)2*6(C6H5CH2)2SO

Guidance literature:

In ethanol; ZrO(ClO4)2 was dissolved in abs. EtOH and 2,2'-dimethoxy propane, mixt.was warmed on a water bath with stirring, ligand was added, mixt. was refluxed for 2-3 h; excess of solvent was distilled off, ppt. was treated with petroleum ether, ppt. was washed and dried in vac.; elem. anal.;

DOI:10.1016/0040-6031(85)85461-7

Reference yield:

zirconiumoxide perchlorate (12591-05-8,15607-09-7) + 4-amino-2,3-dimethyl-1-phenylpyrazolin-5-one (83-07-8) → ZrO(4-aminoantipyrine)3(ClO4)2

Guidance literature:

In methanol; methanolic soln. of Zr-salt was mixed with methanolic soln. of ligand in the required molar ratio, stirred for 2 h; washed with appropriate solvent and finally with ether and dried in a vac. desiccator over P4O10, elem. anal.;

upstream raw materials:

perchloric acid

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