Toluene-3,4-disulfonyl chloride

Base Information

Chemical Name:Toluene-3,4-disulfonyl chloride
CAS No.:26627-38-3
Molecular Formula:C7H6Cl2O4S2
Molecular Weight:289.16
Hs Code.:2904909090
DSSTox Substance ID:DTXSID10347317
Nikkaji Number:J149.769C
Wikidata:Q82121097
Mol file:26627-38-3.mol

Synonyms:Toluene-3,4-disulfonyl chloride;26627-38-3;SCHEMBL2426442;DTXSID10347317;toluene-3,4-disulfonyl di-chloride;4-Methyl-1,2-benzenedisulfonyl dichloride #

Suppliers and Price of Toluene-3,4-disulfonyl chloride

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of Toluene-3,4-disulfonyl chloride

Chemical Property:

PSA：85.04000
LogP:4.01160
XLogP3:2.3
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:2
Exact Mass:287.9084564
Heavy Atom Count:15
Complexity:417

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC1=CC(=C(C=C1)S(=O)(=O)Cl)S(=O)(=O)Cl

Technology Process of Toluene-3,4-disulfonyl chloride

There total 4 articles about Toluene-3,4-disulfonyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 67855-55-4
5-methyl-2-(3-methylbutoxy)-1,3-benzodithiole

: 26627-38-3
4-methylbenzene-1,2-disulfonyl dichloride

Guidance literature:: With water; chlorine; In dichloromethane; tert-butyl alcohol; at 0 - 5 ℃; for 1h;
DOI:10.1016/j.tet.2013.02.053

Reference yield:

: 2941-78-8
2-Amino-5-methylbenzoic acid

: 26627-38-3
4-methylbenzene-1,2-disulfonyl dichloride

Guidance literature:: Multi-step reaction with 2 steps

1: 1,4-dioxane; dichloromethane; i-Amyl alcohol / 1.75 h / 20 - 82 °C

2: chlorine; water / tert-butyl alcohol; dichloromethane / 1 h / 0 - 5 °C

With water; chlorine; In 1,4-dioxane; i-Amyl alcohol; dichloromethane; tert-butyl alcohol;
DOI:10.1016/j.tet.2013.02.053