2-(2-Aminophenyl)-5,6-di-methylbenzimidazole

Base Information

Chemical Name:2-(2-Aminophenyl)-5,6-di-methylbenzimidazole
CAS No.:10173-54-3
Molecular Formula:C₁₅H₁₅N₃
Molecular Weight:237.304
Hs Code.:
DSSTox Substance ID:DTXSID101236873
Mol file:10173-54-3.mol

Synonyms:10173-54-3;2-(2-aminophenyl)-5,6-di-methylbenzimidazole;SCHEMBL12072142;DTXSID101236873;AKOS011620883;2-(5,6-Dimethyl-1H-benzimidazol-2-yl)benzenamine

Suppliers and Price of 2-(2-Aminophenyl)-5,6-di-methylbenzimidazole

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-(2-Aminophenyl)-5,6-di-methylbenzimidazole

Chemical Property:

XLogP3:3.2
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:1
Exact Mass:237.126597491
Heavy Atom Count:18
Complexity:294

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CC2=C(C=C1C)N=C(N2)C3=CC=CC=C3N

Technology Process of 2-(2-Aminophenyl)-5,6-di-methylbenzimidazole

There total 4 articles about 2-(2-Aminophenyl)-5,6-di-methylbenzimidazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 118-48-9
isatoic anhydride

: 3171-45-7
4,5-dimethyl-1,2-phenylenediamine

: 10173-54-3
2-(5,6-dimethyl-1H-benzimidazol-2-yl)-phenylamine

Guidance literature:: With acetic acid; at 90 ℃;
DOI:10.1021/acs.joc.6b02423

Reference yield:

: 6972-71-0
4,5-dimethyl-2-nitrobenzenamine

: 10173-54-3
2-(5,6-dimethyl-1H-benzimidazol-2-yl)-phenylamine

Guidance literature:: Multi-step reaction with 3 steps

1: H₂ / methanol / 2 h / 20 °C / 1551.49 Torr

2: 87 percent / oxone (R) / dimethylformamide / 2 h / 20 °C

3: 93 percent / H₂ / Pd/C / methanol / 2 h / 20 °C / 1551.49 Torr

With Oxone; hydrogen; palladium on activated charcoal; In methanol; N,N-dimethyl-formamide;
DOI:10.1080/00397910701489453

Reference yield:

: 3171-45-7
4,5-dimethyl-1,2-phenylenediamine

: 10173-54-3
2-(5,6-dimethyl-1H-benzimidazol-2-yl)-phenylamine

Guidance literature:: Multi-step reaction with 2 steps

1: 87 percent / oxone (R) / dimethylformamide / 2 h / 20 °C

2: 93 percent / H₂ / Pd/C / methanol / 2 h / 20 °C / 1551.49 Torr

With Oxone; hydrogen; palladium on activated charcoal; In methanol; N,N-dimethyl-formamide;
DOI:10.1080/00397910701489453