2-Fuoro-5-iodo-1,3-dimethylbenzene

Base Information

• Chemical Name: 2-Fuoro-5-iodo-1,3-dimethylbenzene
• CAS No.: 1416549-07-9
• Molecular Formula: C8H8FI
• Molecular Weight: 250.05
• Mol file: 1416549-07-9.mol

Synonyms:2-Fuoro-5-iodo-1,3-dimethylbenzene;2-Fluoro-5-iodo-1,3-dimethylbenzene;1-Iodo-4-fluoro-3,5-dimethylbenzene

Chemical Property of 2-Fuoro-5-iodo-1,3-dimethylbenzene

Chemical Property:

• Boiling Point: 227.3±35.0 °C(Predicted)
• PSA: 0.00000
• Density: 1.686±0.06 g/cm3(Predicted)
• LogP: 3.04710

Purity/Quality:

98%min ^*data from raw suppliers

2-Fluoro-5-iodo-1,3-dimethylbenzene 95+% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-Fuoro-5-iodo-1,3-dimethylbenzene

There total 2 articles about 2-Fuoro-5-iodo-1,3-dimethylbenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-(4-fluoro-3,5-dimethylphenyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane (1147894-98-1) → 2-fluoro-5-iodo-1,3-dimethylbenzene (1416549-07-9)

Guidance literature:

With copper(l) iodide; 1,10-Phenanthroline; potassium iodide; In methanol; water; at 80 ℃; for 1h; High pressure;

DOI:10.1021/ol303164h

Reference yield:

2-fluoro-m-xylene (443-88-9) → 2-fluoro-5-iodo-1,3-dimethylbenzene (1416549-07-9)

Guidance literature:

Multi-step reaction with 2 steps

1: (1,5-cyclooctadiene)(methoxy)iridium(I) dimer; 4,4′-di-(tert-butyl)-2,2′-bipyridyl / tetrahydrofuran / 24 h / 80 °C / High pressure; Inert atmosphere

2: 1,10-Phenanthroline; copper(l) iodide; potassium iodide / methanol; water / 1 h / 80 °C / High pressure

With copper(l) iodide; 1,10-Phenanthroline; (1,5-cyclooctadiene)(methoxy)iridium(I) dimer; 4,4′-di-(tert-butyl)-2,2′-bipyridyl; potassium iodide; In tetrahydrofuran; methanol; water;

DOI:10.1021/ol303164h

upstream raw materials:

2-fluoro-m-xylene

2-(4-fluoro-3,5-dimethylphenyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

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